3-[4-(1,4,7,10,13-pentaoxa-16-aza-cyclooctadec-16-ylmethyl)-phenyl]-1-phenyl-propenone

Base Information

Chemical Name:3-[4-(1,4,7,10,13-pentaoxa-16-aza-cyclooctadec-16-ylmethyl)-phenyl]-1-phenyl-propenone
CAS No.:934161-00-9
Molecular Formula:C₂₈H₃₇NO₆
Molecular Weight:483.605
Hs Code.:

Synonyms:3-[4-(1,4,7,10,13-pentaoxa-16-aza-cyclooctadec-16-ylmethyl)-phenyl]-1-phenyl-propenone

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Chemical Property of 3-[4-(1,4,7,10,13-pentaoxa-16-aza-cyclooctadec-16-ylmethyl)-phenyl]-1-phenyl-propenone

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Technology Process of 3-[4-(1,4,7,10,13-pentaoxa-16-aza-cyclooctadec-16-ylmethyl)-phenyl]-1-phenyl-propenone

There total 3 articles about 3-[4-(1,4,7,10,13-pentaoxa-16-aza-cyclooctadec-16-ylmethyl)-phenyl]-1-phenyl-propenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 934160-98-2
4-(1,4,7,10,13-pentaoxa-16-aza-cyclooctadec-16-ylmethyl)-benzaldehyde

: 98-86-2
acetophenone

: 934161-00-9
3-[4-(1,4,7,10,13-pentaoxa-16-aza-cyclooctadec-16-ylmethyl)-phenyl]-1-phenyl-propenone

Guidance literature:: With sodium hydroxide; In methanol; at 20 ℃; for 15h;
DOI:10.1021/jo062506r

Reference yield:

: 51359-78-5
4-(bromomethyl)benzaldehyde

: 934161-00-9
3-[4-(1,4,7,10,13-pentaoxa-16-aza-cyclooctadec-16-ylmethyl)-phenyl]-1-phenyl-propenone

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / Cs₂CO₃ / acetonitrile / 1.5 h / 80 °C

2: 92 percent / NaOH / methanol / 15 h / 20 °C

With sodium hydroxide; caesium carbonate; In methanol; acetonitrile;
DOI:10.1021/jo062506r

Reference yield:

: 17201-43-3
4-cyanobenzyl bromide

: 934161-00-9
3-[4-(1,4,7,10,13-pentaoxa-16-aza-cyclooctadec-16-ylmethyl)-phenyl]-1-phenyl-propenone

Guidance literature:: Multi-step reaction with 3 steps

1.1: DIBAL-H / toluene / 1 h / 0 °C

1.2: 94 percent / HCl / toluene; H₂O

2.1: 96 percent / Cs₂CO₃ / acetonitrile / 1.5 h / 80 °C

3.1: 92 percent / NaOH / methanol / 15 h / 20 °C

With sodium hydroxide; diisobutylaluminium hydride; caesium carbonate; In methanol; toluene; acetonitrile;
DOI:10.1021/jo062506r