1-bityl-3-methyldiaziridine

Base Information

• Chemical Name: 1-bityl-3-methyldiaziridine
• CAS No.: 26177-38-8
• Molecular Formula: C₆H₁₄N₂
• Molecular Weight: 114.191

Synonyms:1-bityl-3-methyldiaziridine

Chemical Property of 1-bityl-3-methyldiaziridine

Chemical Property:

Purity/Quality:

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Technology Process of 1-bityl-3-methyldiaziridine

There total 2 articles about 1-bityl-3-methyldiaziridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

Acetaldehyd-butylimin (6898-74-4) + O-(2,4-dinitrophenyl)hydroxylamine (17508-17-7) → 2,4-Dinitrophenol (51-28-5) + O-(2,4-dinitrophenyl)acetaldoxime (13181-41-4) + 1-bityl-3-methyldiaziridine (26177-38-8)

Guidance literature:

In dichloromethane; at -30 - -20 ℃; for 3h;

DOI:10.1007/BF00950653

Reference yield: 16.0%

mesityloylacetaldoxime (84298-25-9) + N-butylamine (109-73-9,85404-21-3) → mesitylic acid butylammonium salt (84401-51-4) + acetonitrile (75-05-8,26809-02-9) + 1-bityl-3-methyldiaziridine (26177-38-8)

Guidance literature:

In dichloromethane; Product distribution; 0 deg C, 80 h; 10 deg C, 60 h;

DOI:10.1007/BF00952389

upstream raw materials:

mesityloylacetaldoxime

N-butylamine

Acetaldehyd-butylimin

O-(2,4-dinitrophenyl)hydroxylamine

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