4-(7-(4-(N,N-bis(4-((2-ethylhexyl)oxy)phenyl)amino)phenyl)-9-oxo-9H-fluoren-2-yl)phenylcarbaldehyde

Base Information

Chemical Name:4-(7-(4-(N,N-bis(4-((2-ethylhexyl)oxy)phenyl)amino)phenyl)-9-oxo-9H-fluoren-2-yl)phenylcarbaldehyde
CAS No.:1417779-67-9
Molecular Formula:C₅₄H₅₇NO₄
Molecular Weight:784.051
Hs Code.:

Synonyms:4-(7-(4-(N,N-bis(4-((2-ethylhexyl)oxy)phenyl)amino)phenyl)-9-oxo-9H-fluoren-2-yl)phenylcarbaldehyde

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Chemical Property of 4-(7-(4-(N,N-bis(4-((2-ethylhexyl)oxy)phenyl)amino)phenyl)-9-oxo-9H-fluoren-2-yl)phenylcarbaldehyde

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Technology Process of 4-(7-(4-(N,N-bis(4-((2-ethylhexyl)oxy)phenyl)amino)phenyl)-9-oxo-9H-fluoren-2-yl)phenylcarbaldehyde

There total 3 articles about 4-(7-(4-(N,N-bis(4-((2-ethylhexyl)oxy)phenyl)amino)phenyl)-9-oxo-9H-fluoren-2-yl)phenylcarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.7%

: 1398122-55-8
2-bromo-7-(4-(N,N-bis(4-((2-ethylhexyl)oxy)phenyl)amino)phenyl)-9-oxo-9H-fluorene

: 87199-17-5
4-formylphenylboronic acid,

: 1417779-67-9
4-(7-(4-(N,N-bis(4-((2-ethylhexyl)oxy)phenyl)amino)phenyl)-9-oxo-9H-fluoren-2-yl)phenylcarbaldehyde

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In water; toluene; for 24h; Inert atmosphere; Reflux;

Reference yield:

: 1314556-70-1
4-(2-ethylhexyloxy)-N-(4-(2-ethylhexyloxy)phenyl)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)benzeneamine

: 1417779-67-9
4-(7-(4-(N,N-bis(4-((2-ethylhexyl)oxy)phenyl)amino)phenyl)-9-oxo-9H-fluoren-2-yl)phenylcarbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / toluene; water / 16 h / Inert atmosphere; Reflux

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / toluene; water / 24 h / Inert atmosphere; Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In water; toluene;

Reference yield:

: 1192035-51-0
4-bromo-N,N-bis((4-(2-ethyl)hexyloxy)phenyl)aniline

: 1417779-67-9
4-(7-(4-(N,N-bis(4-((2-ethylhexyl)oxy)phenyl)amino)phenyl)-9-oxo-9H-fluoren-2-yl)phenylcarbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 2.5 h / -78 °C / Inert atmosphere

1.2: -78 °C / Inert atmosphere

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / toluene; water / 16 h / Inert atmosphere; Reflux

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / toluene; water / 24 h / Inert atmosphere; Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; potassium carbonate; In tetrahydrofuran; hexane; water; toluene;