4-(2-ethylhexyloxy)-N-(4-(2-ethylhexyloxy)phenyl)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)benzeneamine

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Chemical Name:4-(2-ethylhexyloxy)-N-(4-(2-ethylhexyloxy)phenyl)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)benzeneamine
CAS No.:1314556-70-1
Molecular Formula:C₄₀H₅₈BNO₄
Molecular Weight:627.716
Hs Code.:

Synonyms:4-(2-ethylhexyloxy)-N-(4-(2-ethylhexyloxy)phenyl)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)benzeneamine

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Chemical Property of 4-(2-ethylhexyloxy)-N-(4-(2-ethylhexyloxy)phenyl)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)benzeneamine

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Technology Process of 4-(2-ethylhexyloxy)-N-(4-(2-ethylhexyloxy)phenyl)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)benzeneamine

There total 4 articles about 4-(2-ethylhexyloxy)-N-(4-(2-ethylhexyloxy)phenyl)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)benzeneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 61676-62-8
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1192035-51-0
4-bromo-N,N-bis((4-(2-ethyl)hexyloxy)phenyl)aniline

: 1314556-70-1
4-(2-ethylhexyloxy)-N-(4-(2-ethylhexyloxy)phenyl)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)benzeneamine

Guidance literature:: 4-bromo-N,N-bis((4-(2-ethyl)hexyloxy)phenyl)aniline; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 2.5h; Inert atmosphere;

2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; In tetrahydrofuran; hexane; at -78 ℃; Inert atmosphere;

Reference yield:

: 540-38-5
p-Iodophenol

: 1314556-70-1
4-(2-ethylhexyloxy)-N-(4-(2-ethylhexyloxy)phenyl)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)benzeneamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 50 h / 100 °C / Inert atmosphere

2.1: 1,10-Phenanthroline / toluene / 100 °C / Inert atmosphere

2.2: 12 h / 120 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -80 - 20 °C / Inert atmosphere

3.2: 12 h / -80 - 20 °C / Inert atmosphere

With n-butyllithium; 1,10-Phenanthroline; potassium carbonate; In tetrahydrofuran; hexane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.materresbull.2015.06.026

Reference yield:

: 259111-27-8
(4-[(2-ethylhexyl)oxy]-1-iodobenzene)

: 1314556-70-1
4-(2-ethylhexyloxy)-N-(4-(2-ethylhexyloxy)phenyl)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)benzeneamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,10-Phenanthroline / toluene / 100 °C / Inert atmosphere

1.2: 12 h / 120 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -80 - 20 °C / Inert atmosphere

2.2: 12 h / -80 - 20 °C / Inert atmosphere

With n-butyllithium; 1,10-Phenanthroline; In tetrahydrofuran; hexane; toluene;
DOI:10.1016/j.materresbull.2015.06.026