(R)-N-tert-butoxy-N-1'-(1''-naphthyl)ethyl (S)-2-(4'''-methoxybenzyloxy)heptanamide

Base Information

Chemical Name:(R)-N-tert-butoxy-N-1'-(1''-naphthyl)ethyl (S)-2-(4'''-methoxybenzyloxy)heptanamide
CAS No.:1234714-11-4
Molecular Formula:C₃₁H₄₁NO₄
Molecular Weight:491.671
Hs Code.:

Synonyms:(R)-N-tert-butoxy-N-1'-(1''-naphthyl)ethyl (S)-2-(4'''-methoxybenzyloxy)heptanamide

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Chemical Property of (R)-N-tert-butoxy-N-1'-(1''-naphthyl)ethyl (S)-2-(4'''-methoxybenzyloxy)heptanamide

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Technology Process of (R)-N-tert-butoxy-N-1'-(1''-naphthyl)ethyl (S)-2-(4'''-methoxybenzyloxy)heptanamide

There total 1 articles about (R)-N-tert-butoxy-N-1'-(1''-naphthyl)ethyl (S)-2-(4'''-methoxybenzyloxy)heptanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 628-17-1
amyl iodide

: 1234713-89-3
(R)-N-tert-butoxy-N-1'-(1''-naphthyl)ethyl 2-(4'''-methoxybenzyloxy)acetamide

: 1234714-11-4
(R)-N-tert-butoxy-N-1'-(1''-naphthyl)ethyl (S)-2-(4'''-methoxybenzyloxy)heptanamide

Guidance literature:: (R)-N-tert-butoxy-N-1'-(1''-naphthyl)ethyl 2-(4'''-methoxybenzyloxy)acetamide; With 18-crown-6 ether; potassium hexamethylsilazane; In tetrahydrofuran; at -78 ℃; Inert atmosphere;

amyl iodide; In tetrahydrofuran; at -78 ℃; optical yield given as %de; diastereoselective reaction;
DOI:10.1016/j.tet.2010.03.105

Reference yield: 100.0%

: 1234714-11-4
(R)-N-tert-butoxy-N-1'-(1''-naphthyl)ethyl (S)-2-(4'''-methoxybenzyloxy)heptanamide

: 1177266-32-8
C₁₆H₂₁NO

: (S)-2-(4-Methoxy-benzyloxy)-heptanal

Guidance literature:: (R)-N-tert-butoxy-N-1'-(1''-naphthyl)ethyl (S)-2-(4'''-methoxybenzyloxy)heptanamide; With lithium aluminium tetrahydride; In tetrahydrofuran; at -15 ℃; Inert atmosphere;

In tetrahydrofuran; at 0 ℃; pH=7; phosphate buffer;
DOI:10.1016/j.tet.2010.03.105