Boc-Tyr(Mtb)-Gly-Gly-Phe-Met-OMtb

Base Information

Chemical Name:Boc-Tyr(Mtb)-Gly-Gly-Phe-Met-OMtb
CAS No.:129398-74-9
Molecular Formula:C₄₈H₅₉N₅O₉S₃
Molecular Weight:946.223
Hs Code.:

Synonyms:Boc-Tyr(Mtb)-Gly-Gly-Phe-Met-OMtb

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Chemical Property of Boc-Tyr(Mtb)-Gly-Gly-Phe-Met-OMtb

Chemical Property:

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Technology Process of Boc-Tyr(Mtb)-Gly-Gly-Phe-Met-OMtb

There total 12 articles about Boc-Tyr(Mtb)-Gly-Gly-Phe-Met-OMtb which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 129398-73-8
Boc-Tyr(Msib)-Gly-Gly-Phe-Met(O)-OMsib

: 129398-74-9
Boc-Tyr(Mtb)-Gly-Gly-Phe-Met-OMtb

Guidance literature:: With pyridine; sulfur trioxide; ethane-1,2-dithiol; N,N-dimethyl-formamide; at 20 ℃; for 1h;

Reference yield:

: 3446-90-0
4-(methylthio)benzyl alcohol

: 129398-74-9
Boc-Tyr(Mtb)-Gly-Gly-Phe-Met-OMtb

Guidance literature:: Multi-step reaction with 12 steps

1: 99 percent / trimethylsilyl bromide / CHCl₃ / 1 h / 0 °C

2: 75 percent / 30percent H₂O₂ / acetic acid / 20 h / 20 °C

3: 62 percent / dicyclohexylamine / dimethylformamide

4: TFA, anisole

5: 81 percent / Et₃N, N-methylmorpholine / dimethylformamide / 3 h

6: TFA, anisole

7: 98 percent / Et₃N, N-methylmorpholine / dimethylformamide / 3 h

8: TFA, anisole

9: 83 percent / Et₃N, N-methylmorpholine / 3 h

10: TFA, anisole

11: 68 percent / Et₃N, N-methylmorpholine / dimethylformamide

12: 88 percent / DMF/SO₃, ethane-1,2-dithiol, pyridine / 1 h / 20 °C

With 4-methyl-morpholine; pyridine; trimethylsilyl bromide; sulfur trioxide; dihydrogen peroxide; ethane-1,2-dithiol; methoxybenzene; triethylamine; N,N-dimethyl-formamide; N-cyclohexyl-cyclohexanamine; trifluoroacetic acid; In chloroform; acetic acid; N,N-dimethyl-formamide;

Reference yield:

: 38185-19-2
4-(methylthio)benzyl bromide

: 129398-74-9
Boc-Tyr(Mtb)-Gly-Gly-Phe-Met-OMtb

Guidance literature:: Multi-step reaction with 11 steps

1: 75 percent / 30percent H₂O₂ / acetic acid / 20 h / 20 °C

2: 62 percent / dicyclohexylamine / dimethylformamide

3: TFA, anisole

4: 81 percent / Et₃N, N-methylmorpholine / dimethylformamide / 3 h

5: TFA, anisole

6: 98 percent / Et₃N, N-methylmorpholine / dimethylformamide / 3 h

7: TFA, anisole

8: 83 percent / Et₃N, N-methylmorpholine / 3 h

9: TFA, anisole

10: 68 percent / Et₃N, N-methylmorpholine / dimethylformamide

11: 88 percent / DMF/SO₃, ethane-1,2-dithiol, pyridine / 1 h / 20 °C

With 4-methyl-morpholine; pyridine; sulfur trioxide; dihydrogen peroxide; ethane-1,2-dithiol; methoxybenzene; triethylamine; N,N-dimethyl-formamide; N-cyclohexyl-cyclohexanamine; trifluoroacetic acid; In acetic acid; N,N-dimethyl-formamide;