C₇H₄BrF₂⁽¹⁸⁾F

Base Information

Chemical Name:C₇H₄BrF₂⁽¹⁸⁾F
CAS No.:1456616-01-5
Molecular Formula:C₇H₄BrF₃
Molecular Weight:224.01
Hs Code.:

C<sub>7</sub>H<sub>4</sub>BrF<sub>2</sub><sup>(18)</sup>F

Synonyms:C₇H₄BrF₂⁽¹⁸⁾F

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₇H₄BrF₂⁽¹⁸⁾F

Chemical Property:

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Technology Process of C₇H₄BrF₂⁽¹⁸⁾F

There total 8 articles about C₇H₄BrF₂⁽¹⁸⁾F which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1456616-01-5
C₇H₄BrF₂⁽¹⁸⁾F

Guidance literature:: In N,N-dimethyl-formamide; at 20 ℃; for 0.166667h; Sealed tube;

Reference yield:

: 1514-87-0
metyhyl chlorodifluoroacetate

: 589-87-7
1,4-bromoiodobenzene

: 1456616-01-5
C₇H₄BrF₂⁽¹⁸⁾F

Guidance literature:: With copper(l) iodide; 4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]hexacosan/[18F]fluoride; N,N,N,N,-tetramethylethylenediamine; In N,N-dimethyl-formamide; acetonitrile; at 100 - 150 ℃; for 0.333333h; regioselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1038/nchem.1756

Reference yield:

: 51776-71-7
p-bromo-α,α-difluorotoluene

: 1456616-01-5
C₇H₄BrF₂⁽¹⁸⁾F

Guidance literature:: p-bromo-α,α-difluorotoluene; With 18-crown-6 ether; (+/-)-(1S,2S)-[1,2-cyclohexanediamino-N,N'-bis(3,5-di-t-butylsalicylidene)]manganese (III) chloride; silver trifluoromethanesulfonate; potassium carbonate; [18F]fluoride ion, cyclotron produced, NCA; In acetonitrile; at 60 ℃; for 0.0833333h; Inert atmosphere;

With iodosylbenzene; In acetonitrile; at 60 ℃; for 0.416667h; Inert atmosphere;
DOI:10.1039/c4cc05762g