benzyl 4-<<2,6-dimethyl-4-(phenylmethoxy)phenyl>-methyl>-4-methyl-5-oxo-2-phenyl-3-oxazolidinecarboxylate

Base Information

Chemical Name:benzyl 4-<<2,6-dimethyl-4-(phenylmethoxy)phenyl>-methyl>-4-methyl-5-oxo-2-phenyl-3-oxazolidinecarboxylate
CAS No.:111648-86-3
Molecular Formula:C₃₄H₃₃NO₅
Molecular Weight:535.64
Hs Code.:

Synonyms:benzyl 4-<<2,6-dimethyl-4-(phenylmethoxy)phenyl>-methyl>-4-methyl-5-oxo-2-phenyl-3-oxazolidinecarboxylate

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Chemical Property of benzyl 4-<<2,6-dimethyl-4-(phenylmethoxy)phenyl>-methyl>-4-methyl-5-oxo-2-phenyl-3-oxazolidinecarboxylate

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Technology Process of benzyl 4-<<2,6-dimethyl-4-(phenylmethoxy)phenyl>-methyl>-4-methyl-5-oxo-2-phenyl-3-oxazolidinecarboxylate

There total 9 articles about benzyl 4-<<2,6-dimethyl-4-(phenylmethoxy)phenyl>-methyl>-4-methyl-5-oxo-2-phenyl-3-oxazolidinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: ethyl acetate n-hexane

: 111648-85-2
benzyl 4-<<2,6-dimethyl-4-(phenylmethoxy)phenyl>-methyl>-5-oxo-2-phenyl-3-oxazolidinecarboxylate

: 74-88-4
methyl iodide

: 111648-86-3
benzyl 4-<<2,6-dimethyl-4-(phenylmethoxy)phenyl>-methyl>-4-methyl-5-oxo-2-phenyl-3-oxazolidinecarboxylate

Guidance literature:: With potassium hydrogensulfate; N₂; potassium; In tetrahydrofuran; toluene;

Reference yield:

: 100-52-7
benzaldehyde

: 111648-86-3
benzyl 4-<<2,6-dimethyl-4-(phenylmethoxy)phenyl>-methyl>-4-methyl-5-oxo-2-phenyl-3-oxazolidinecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / p-toluenesulfonic acid monohydrate / 1,1,1-trichloro-ethane / 16 h / Heating

2: 1.) potassium hexamethyldisilazane / 1.) toluene, DMF, a) 30 min, b) RT, 30 min, 2.) toluene, DMF, RT, 3 h

With potassium hexamethyldisilazane; toluene-4-sulfonic acid; In 1,1,1-trichloroethane;

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 111648-86-3
benzyl 4-<<2,6-dimethyl-4-(phenylmethoxy)phenyl>-methyl>-4-methyl-5-oxo-2-phenyl-3-oxazolidinecarboxylate

Guidance literature:: Multi-step reaction with 6 steps

1: 10percent aq. NaOH / H₂O / 2 h

2: K₂CO₃ / dimethylformamide / 16 h / Ambient temperature

3: 1.) sodium hydride / 1.) DMF, 10 min, 2.) DMF, 16 h

4: 92 percent / aq. NaOH / methanol / 3 h

5: 68 percent / p-toluenesulfonic acid monohydrate / 1,1,1-trichloro-ethane / 16 h / Heating

6: 1.) potassium hexamethyldisilazane / 1.) toluene, DMF, a) 30 min, b) RT, 30 min, 2.) toluene, DMF, RT, 3 h

With sodium hydroxide; potassium hexamethyldisilazane; sodium hydride; potassium carbonate; toluene-4-sulfonic acid; In methanol; 1,1,1-trichloroethane; water; N,N-dimethyl-formamide;