(E)-trisylhydrazone de la cyclopentylidene-2 cyclopentanone-1

Base Information

• Chemical Name: (E)-trisylhydrazone de la cyclopentylidene-2 cyclopentanone-1
• CAS No.: 104703-62-0
• Molecular Formula: C₂₅H₃₈N₂O₂S
• Molecular Weight: 430.655

Synonyms:(E)-trisylhydrazone de la cyclopentylidene-2 cyclopentanone-1

Chemical Property of (E)-trisylhydrazone de la cyclopentylidene-2 cyclopentanone-1

Chemical Property:

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Technology Process of (E)-trisylhydrazone de la cyclopentylidene-2 cyclopentanone-1

There total 1 articles about (E)-trisylhydrazone de la cyclopentylidene-2 cyclopentanone-1 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

trisylhydrazine (39085-59-1) + 2-cyclopentylidenecyclopentan-1-one (825-25-2) → (E)-trisylhydrazone de la cyclopentylidene-2 cyclopentanone-1 (104703-62-0)

Guidance literature:

With hydrogenchloride; In methanol; 1.) room temp., 2.) in a refrigerator, overnight;

Reference yield: 66.0%

2-iodo-1-methoxyethane (4296-15-5) + (E)-trisylhydrazone de la cyclopentylidene-2 cyclopentanone-1 (104703-62-0) → trisylhydrazone de la cyclopentenyl-2 (methoxy-2 ethyl)-2 cyclopentanone-1 (104703-54-0)

Guidance literature:

With sec.-butyllithium; In tetrahydrofuran; cyclohexane; 1.) -78 deg C, 1.5 h, 2.) -78 deg C, 7 h;

Reference yield: 54.0%

Dimethyldisulphide (624-92-0) + (E)-trisylhydrazone de la cyclopentylidene-2 cyclopentanone-1 (104703-62-0) → trisylhydrazone de la cyclopentenyl-2 methylthio-2 cyclopentanone-1 (104703-53-9)

Guidance literature:

With sec.-butyllithium; In tetrahydrofuran; cyclohexane; 1.) -78 deg C, 1.5 h, 2.) -78 deg C, 7 h;

upstream raw materials:

trisylhydrazine

2-cyclopentylidenecyclopentan-1-one

Downstream raw materials:

trisylhydrazone de la cyclopentenyl-2 methylthio-2 cyclopentanone-1

trisylhydrazone de la cyclopentenyl-2 (methoxy-2 ethyl)-2 cyclopentanone-1

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