6-deoxy-6-iodo-2,3-O-isopropylidene-4-O-methyl-1-O-tosyl-β-D-fructofuranose

Base Information

Chemical Name:6-deoxy-6-iodo-2,3-O-isopropylidene-4-O-methyl-1-O-tosyl-β-D-fructofuranose
CAS No.:152035-17-1
Molecular Formula:C₁₇H₂₃IO₇S
Molecular Weight:498.336
Hs Code.:

Synonyms:6-deoxy-6-iodo-2,3-O-isopropylidene-4-O-methyl-1-O-tosyl-β-D-fructofuranose

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Chemical Property of 6-deoxy-6-iodo-2,3-O-isopropylidene-4-O-methyl-1-O-tosyl-β-D-fructofuranose

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Technology Process of 6-deoxy-6-iodo-2,3-O-isopropylidene-4-O-methyl-1-O-tosyl-β-D-fructofuranose

There total 2 articles about 6-deoxy-6-iodo-2,3-O-isopropylidene-4-O-methyl-1-O-tosyl-β-D-fructofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 152035-16-0
2,3-O-Isopropylidene-4-O-methyl-1,6-di-O-tosyl-β-D-fructofuranose

: 1,6-dideoxy-1,6-diiodo-2,3-O-isopropylidene-4-O-methyl-β-D-fructofuranose

: 152035-17-1
6-deoxy-6-iodo-2,3-O-isopropylidene-4-O-methyl-1-O-tosyl-β-D-fructofuranose

Guidance literature:: With sodium iodide; In acetone; at 90 - 100 ℃; for 12h;

Reference yield:

: 32087-60-8
2,3-O-isopropylidene-1,6-bis-O-(p-tolylsulphonyl)-β-D-fructofuranose

: 152035-17-1
6-deoxy-6-iodo-2,3-O-isopropylidene-4-O-methyl-1-O-tosyl-β-D-fructofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / Ag₂O / dimethylformamide / 20 h / 25 °C

2: 91 percent / NaI / acetone / 12 h / 90 - 100 °C

With sodium iodide; silver(l) oxide; In N,N-dimethyl-formamide; acetone;