AC-3,5-DINITRO-TYR-OET

Base Information

• Chemical Name: AC-3,5-DINITRO-TYR-OET
• CAS No.: 29358-99-4
• Molecular Formula: C13H15 N3 O8
• Molecular Weight: 341.27
• Hs Code.: 2924299090
• Mol file: 29358-99-4.mol

Synonyms:Tyrosine,N-acetyl-3,5-dinitro-, ethyl ester (8CI); 3,5-Dinitro-N-acetyl-L-tyrosine ethylester; N-Acetyl-3,5-dinitro-L-tyrosine ethyl ester

Chemical Property of AC-3,5-DINITRO-TYR-OET

Chemical Property:

• Vapor Pressure: 0-0Pa at 20-25℃
• PSA: 167.27000
• Density: 1.413 at 20℃
• LogP: 2.25620
• Storage Temp.: −20°C

Purity/Quality:

99% ^*data from raw suppliers

AC-3,5-Dinitro-Tyr-OEt ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of AC-3,5-DINITRO-TYR-OET

There total 6 articles about AC-3,5-DINITRO-TYR-OET which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3.5-Dinitro-N-acetyl-L-tyrosin (20767-00-4) → N-acetyl-3,5-dinitro-L-tyrosine ethyl ester (29358-99-4)

Guidance literature:

With thionyl chloride; benzene; Erwaermen des Reaktionsprodukts mit Aethanol;

DOI:10.1021/jo01129a014

Reference yield:

N-acetyl-L-tyrosine (537-55-3) → N-acetyl-3,5-dinitro-L-tyrosine ethyl ester (29358-99-4)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid; concentrated H₂SO₄; concentrated aqueous HNO₃

2: SOCl₂; benzene / Erwaermen des Reaktionsprodukts mit Aethanol

With thionyl chloride; sulfuric acid; nitric acid; acetic acid; benzene;

DOI:10.1021/jo01129a014

Reference yield:

NSC 80662 (17360-11-1) → N-acetyl-3,5-dinitro-L-tyrosine ethyl ester (29358-99-4)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. NaOH solution

2: toluene-sulfonic acid-⁽⁴⁾

With sodium hydroxide; toluene-4-sulfonic acid;

upstream raw materials:

ethanol

3.5-Dinitro-N-acetyl-L-tyrosin

L-tyrosine

acetyl chloride

Downstream raw materials:

N-Acetyl-3-<4-(3-tert-butyl-4-hydroxy-phenoxy)-3,5-dinitro-phenyl>-L-alanin-aethylester

N-Acetyl-3,5-dinitro-L-tyrosinaethylester-4'-methyl-2'-methoxyphenylaether

N-Acetyl-3,5-diiod-L-tyrosinaethylester-4'-acetamido-1'-naphthylaether

N-Acetyl-3,5-diiod-L-tyrosinaethylester-7'-methoxy-1'-naphthylaether