Benzene,1,3,5-trifluoro-2,4,6-trinitro-

Base Information

• Chemical Name: Benzene,1,3,5-trifluoro-2,4,6-trinitro-
• CAS No.: 1423-11-6
• Molecular Formula: C6F3 N3 O6
• Molecular Weight: 267.078
• Mol file: 1423-11-6.mol

Synonyms:1,3,5-Trifluorotrinitrobenzene

Chemical Property of Benzene,1,3,5-trifluoro-2,4,6-trinitro-

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s): 3
• Hazard Codes: 3:
• Safety Statements: Reacts with hydrazine to form"> − and NOx. See also NITRO COMPOUNDS of AROMATIC HYDROCARBONS and FLUORIDES." target="_blank">Reacts with hydrazine to form

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzene,1,3,5-trifluoro-2,4,6-trinitro-

There total 4 articles about Benzene,1,3,5-trifluoro-2,4,6-trinitro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4,6-trifluoro-1,3-dinitrobenzene (392-51-8) → 1,3,5-trifluoro-2,4,6-trinitrobenzene (1423-11-6)

Guidance literature:

With sulfuric acid; sulfur trioxide; potassium nitrate; at 163 ℃;

DOI:10.1021/jo01070a525

Reference yield:

2,4,6-trichloronitrobenzene (18708-70-8) → 1,3,5-trifluoro-2,4,6-trinitrobenzene (1423-11-6)

Guidance literature:

Multi-step reaction with 3 steps

1: KF / dimethylsulfoxide

2: NO₂/HNO₃, SO₃/H₂SO₄ / 100 °C

3: KNO₃, SO₃/H₂SO₄ / 163 °C

With potassium fluoride; sulfuric acid; sulfur trioxide; nitric acid; Nitrogen dioxide; potassium nitrate; In dimethyl sulfoxide;

DOI:10.1021/jo01070a525

Reference yield:

1,3,5-trifluoro-2-nitrobenzene (315-14-0) → 1,3,5-trifluoro-2,4,6-trinitrobenzene (1423-11-6)

Guidance literature:

Multi-step reaction with 2 steps

1: NO₂/HNO₃, SO₃/H₂SO₄ / 100 °C

2: KNO₃, SO₃/H₂SO₄ / 163 °C

With sulfuric acid; sulfur trioxide; nitric acid; Nitrogen dioxide; potassium nitrate;

DOI:10.1021/jo01070a525

upstream raw materials:

2,4,6-trifluoro-1,3-dinitrobenzene

1,3,5-trifluoro-2-nitrobenzene

2,4,6-trichloronitrobenzene

Downstream raw materials:

1,3-Diacetamido-5-fluoro-2,4,6-trinitrobenzene

1-acetylamino-3,5-difluorotrinitrobenzene

2,4,6-triamino-1,3,5-trinitrobenzene

1-amino-3,5-difluorotrinitrobenzene