N-[2-t-butyl-5-(4-cyclohexyl-3-hydroxybutyl)phenyl]-2-(9H-xanthen-9-yl)acetamide

Base Information

• Chemical Name: N-[2-t-butyl-5-(4-cyclohexyl-3-hydroxybutyl)phenyl]-2-(9H-xanthen-9-yl)acetamide
• CAS No.: 168621-95-2
• Molecular Formula: C₃₅H₄₃NO₃
• Molecular Weight: 525.731

Synonyms:N-[2-t-butyl-5-(4-cyclohexyl-3-hydroxybutyl)phenyl]-2-(9H-xanthen-9-yl)acetamide

Chemical Property of N-[2-t-butyl-5-(4-cyclohexyl-3-hydroxybutyl)phenyl]-2-(9H-xanthen-9-yl)acetamide

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Technology Process of N-[2-t-butyl-5-(4-cyclohexyl-3-hydroxybutyl)phenyl]-2-(9H-xanthen-9-yl)acetamide

There total 1 articles about N-[2-t-butyl-5-(4-cyclohexyl-3-hydroxybutyl)phenyl]-2-(9H-xanthen-9-yl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

N-[2-t-butyl-5-(3-oxopropyl)phenyl]-2-(9H-xanthen-9-yl)acetamide (168624-86-0) + cyclohexylmethyl magnesium bromide (35166-78-0) → N-[2-t-butyl-5-(4-cyclohexyl-3-hydroxybutyl)phenyl]-2-(9H-xanthen-9-yl)acetamide (168621-95-2)

Guidance literature:

With ammonium chloride; In tetrahydrofuran; diethyl ether;

Reference yield: 96.0%

N-[2-t-butyl-5-(4-cyclohexyl-3-hydroxybutyl)phenyl]-2-(9H-xanthen-9-yl)acetamide (168621-95-2) + benzyl glycolate (30379-58-9) + trichloromethyl chloroformate (503-38-8) → N-{2-t-butyl-5-[3-(benzyloxycarbonyl)-methoxycarbonyloxy-4-cyclohexylbutyl)phenyl]-2-(9H-xanthen-9-yl)acetamide

Guidance literature:

With pyridine; dmap; sodium chloride; In tetrahydrofuran; dichloromethane;

Reference yield: 84.0%

succinic acid anhydride (108-30-5) + N-[2-t-butyl-5-(4-cyclohexyl-3-hydroxybutyl)phenyl]-2-(9H-xanthen-9-yl)acetamide (168621-95-2) → 1-(2-{4-t-butyl-3-[2-(9H-xanthen-9-yl)acetamido]phenyl}ethyl)-2-cyclohexylethyl hydrogen succinate

Guidance literature:

With pyridine; dmap; In 5,5-dimethyl-1,3-cyclohexadiene;

upstream raw materials:

N-[2-t-butyl-5-(3-oxopropyl)phenyl]-2-(9H-xanthen-9-yl)acetamide

cyclohexylmethyl magnesium bromide

Downstream raw materials:

N-[2-t-butyl-5-(5-cyclohexyl-3-oxopentyl)phenyl]-2-(9H-xanthen-9-yl)acetamide

N-[2-t-Butyl-5-(4-cyclohexyl-3-carbamoyloxybutyl)-phenyl]-2-(9H-xanthen-9-yl)acetamide

α-1-(2-{4-t-Butyl-3-[2-(9H-xanthen-9-yl)-acetamido]phenyl}ethyl)-2-cyclohexylethyl 4-(morpholinomethyl)benzoate

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