(S)-methyl 2-{ N-[2-(3-benzyloxyphenyl)ethyl]-N-(p-tosyl)amino}propionate

Base Information

Chemical Name:(S)-methyl 2-{ N-[2-(3-benzyloxyphenyl)ethyl]-N-(p-tosyl)amino}propionate
CAS No.:1253197-64-6
Molecular Formula:C₂₆H₂₉NO₅S
Molecular Weight:467.586
Hs Code.:

Synonyms:(S)-methyl 2-{ N-[2-(3-benzyloxyphenyl)ethyl]-N-(p-tosyl)amino}propionate

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Chemical Property of (S)-methyl 2-{ N-[2-(3-benzyloxyphenyl)ethyl]-N-(p-tosyl)amino}propionate

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Technology Process of (S)-methyl 2-{ N-[2-(3-benzyloxyphenyl)ethyl]-N-(p-tosyl)amino}propionate

There total 4 articles about (S)-methyl 2-{ N-[2-(3-benzyloxyphenyl)ethyl]-N-(p-tosyl)amino}propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 177259-98-2
2-[(3-(benzyloxy)phenyl)]ethan-1-ol

: 59724-69-5
(S)-N-tosylalanine methyl ester

: 1253197-64-6
(S)-methyl 2-{ N-[2-(3-benzyloxyphenyl)ethyl]-N-(p-tosyl)amino}propionate

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; for 17h; Inert atmosphere;
DOI:10.1021/acs.jmedchem.5b00897

Reference yield:

: 13398-94-2
2-(3-hydroxyphenyl)ethanol

: 1253197-64-6
(S)-methyl 2-{ N-[2-(3-benzyloxyphenyl)ethyl]-N-(p-tosyl)amino}propionate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / 0.67 h / 100 °C / 3000.3 Torr / Microwave irradiation

2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 17 h / 0 - 20 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In tetrahydrofuran;
DOI:10.1021/acs.jmedchem.5b00897

Reference yield:

: 100-39-0
benzyl bromide

: 1253197-64-6
(S)-methyl 2-{ N-[2-(3-benzyloxyphenyl)ethyl]-N-(p-tosyl)amino}propionate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / 0.67 h / 100 °C / 3000.3 Torr / Microwave irradiation

2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 17 h / 0 - 20 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In tetrahydrofuran;
DOI:10.1021/acs.jmedchem.5b00897