methyl 4,6-O-cyclohexylidene-2,3-di-O-(benzyl-d7)-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:methyl 4,6-O-cyclohexylidene-2,3-di-O-(benzyl-d7)-1-thio-β-D-glucopyranoside
CAS No.:854735-94-7
Molecular Formula:C₂₇H₃₄O₅S
Molecular Weight:484.519
Hs Code.:

Synonyms:methyl 4,6-O-cyclohexylidene-2,3-di-O-(benzyl-d7)-1-thio-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4,6-O-cyclohexylidene-2,3-di-O-(benzyl-d7)-1-thio-β-D-glucopyranoside

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Technology Process of methyl 4,6-O-cyclohexylidene-2,3-di-O-(benzyl-d7)-1-thio-β-D-glucopyranoside

There total 2 articles about methyl 4,6-O-cyclohexylidene-2,3-di-O-(benzyl-d7)-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 854735-98-1
methyl 4,6-O-cyclohexylidene-1-thio-β-D-glucopyranoside

: 35656-93-0
perdeuteriobenzyl bromide

: 854735-94-7
methyl 4,6-O-cyclohexylidene-2,3-di-O-(benzyl-d7)-1-thio-β-D-glucopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 8h;
DOI:10.1016/j.tet.2007.10.087

Reference yield:

: 933-40-4
cycloxexanone dimethyl ketal

: 35656-93-0
perdeuteriobenzyl bromide

: 124-41-4
sodium methylate

: 13350-45-3
methyl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranoside

: 854735-94-7
methyl 4,6-O-cyclohexylidene-2,3-di-O-(benzyl-d7)-1-thio-β-D-glucopyranoside

Guidance literature:: sodium methylate; methyl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranoside;

cycloxexanone dimethyl ketal; With camphor-10-sulfonic acid;

perdeuteriobenzyl bromide; With sodium hydride;
DOI:10.1016/j.tetlet.2005.03.066

Reference yield:

: 854735-94-7
methyl 4,6-O-cyclohexylidene-2,3-di-O-(benzyl-d7)-1-thio-β-D-glucopyranoside

: 4-methoxyphenyl 3-O-(benzyl-d7)-4,6-O-cyclohexylidene-β-D-glucopyranoside

: 4-methoxyphenyl 4,6-O-cyclohexylidene-2,3-di-O-(benzyl-d7)-α-D-glucopyranosyl-(1->2)-3-O-(benzyl-d7)-4,6-O-cyclohexylidene-β-D-glucopyranoside

: C₅₂⁽²⁾H₂₁H₄₁O₁₂

Guidance literature:: With 2,6-di-tert-butyl-4-methylpyridine; methyl trifluoromethanesulfonate; In 1,2-dichloro-ethane; at 20 ℃; for 24h;
DOI:10.1016/j.tet.2007.10.087