C₂₆H₂₂FN₃O₄

Base Information

Chemical Name:C₂₆H₂₂FN₃O₄
CAS No.:1380111-65-8
Molecular Formula:C₂₆H₂₂FN₃O₄
Molecular Weight:459.477
Hs Code.:

C<sub>26</sub>H<sub>22</sub>FN<sub>3</sub>O<sub>4</sub>

Synonyms:C₂₆H₂₂FN₃O₄

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Chemical Property of C₂₆H₂₂FN₃O₄

Chemical Property:

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Technology Process of C₂₆H₂₂FN₃O₄

There total 8 articles about C₂₆H₂₂FN₃O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 403-45-2
6-fluoronicotinic acid

: 1380112-29-7
CH₄O₃S*C₂₀H₂₀N₂O₃

: 1380111-65-8
C₂₆H₂₂FN₃O₄

Guidance literature:: 6-fluoronicotinic acid; With 1,1'-carbonyldiimidazole; In N,N-dimethyl acetamide; at 20 - 25 ℃; for 0.25h;

CH₄O₃S*C₂₀H₂₀N₂O₃; With triethylamine; In N,N-dimethyl acetamide; at 20 - 25 ℃; for 5h;

Reference yield:

: 100-39-0
benzyl bromide

: 1380111-65-8
C₂₆H₂₂FN₃O₄

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hydroxide / methanol; water / Reflux

2.1: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 60 °C

3.1: potassium carbonate / dimethyl sulfoxide / 1 h / 20 - 25 °C

4.1: triethylamine / dichloromethane / 1 h / 0 °C

5.1: potassium iodide / N,N-dimethyl-formamide / 20 - 25 °C

6.1: hydrazine hydrate / ethanol / 1 h / Reflux

7.1: water; ethyl acetate / 20 - 50 °C

8.1: 1,1'-carbonyldiimidazole / N,N-dimethyl acetamide / 0.25 h / 20 - 25 °C

8.2: 5 h / 20 - 25 °C

With hydroxylamine hydrochloride; sodium acetate; potassium carbonate; hydrazine hydrate; triethylamine; 1,1'-carbonyldiimidazole; potassium iodide; sodium hydroxide; In methanol; ethanol; dichloromethane; N,N-dimethyl acetamide; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 501-30-4,123712-78-7
5-hydroxy-2-(hydroxymethyl)-4H-pyran-4-one

: 1380111-65-8
C₂₆H₂₂FN₃O₄

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hydroxide / methanol; water / Reflux

2.1: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 60 °C

3.1: potassium carbonate / dimethyl sulfoxide / 1 h / 20 - 25 °C

4.1: triethylamine / dichloromethane / 1 h / 0 °C

5.1: potassium iodide / N,N-dimethyl-formamide / 20 - 25 °C

6.1: hydrazine hydrate / ethanol / 1 h / Reflux

7.1: water; ethyl acetate / 20 - 50 °C

8.1: 1,1'-carbonyldiimidazole / N,N-dimethyl acetamide / 0.25 h / 20 - 25 °C

8.2: 5 h / 20 - 25 °C

With hydroxylamine hydrochloride; sodium acetate; potassium carbonate; hydrazine hydrate; triethylamine; 1,1'-carbonyldiimidazole; potassium iodide; sodium hydroxide; In methanol; ethanol; dichloromethane; N,N-dimethyl acetamide; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;