(S)-3-(4-(2-amino-6-chloropyrimidin-4-yl)phenyl)-2-(tert-butoxycarbonylamino)propanoic acid, tert-butylamine salt

Base Information

Chemical Name:(S)-3-(4-(2-amino-6-chloropyrimidin-4-yl)phenyl)-2-(tert-butoxycarbonylamino)propanoic acid, tert-butylamine salt
CAS No.:1116460-10-6
Molecular Formula:C₄H₁₁N*C₁₈H₂₁ClN₄O₄
Molecular Weight:465.98
Hs Code.:

Synonyms:(S)-3-(4-(2-amino-6-chloropyrimidin-4-yl)phenyl)-2-(tert-butoxycarbonylamino)propanoic acid, tert-butylamine salt

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Chemical Property of (S)-3-(4-(2-amino-6-chloropyrimidin-4-yl)phenyl)-2-(tert-butoxycarbonylamino)propanoic acid, tert-butylamine salt

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Technology Process of (S)-3-(4-(2-amino-6-chloropyrimidin-4-yl)phenyl)-2-(tert-butoxycarbonylamino)propanoic acid, tert-butylamine salt

There total 3 articles about (S)-3-(4-(2-amino-6-chloropyrimidin-4-yl)phenyl)-2-(tert-butoxycarbonylamino)propanoic acid, tert-butylamine salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1033804-86-2
(S)-3-[4-(2-amino-6-chloropyrimidin-4-yl)phenyl]-2-{[(tert-butoxy)carbonyl]amino}propanoic acid

: C₂₂H₂₃Cl₂N₇O₄

: 1125828-47-8
C₃₂H₃₉N₅O₈

: 75-64-9
tert-butylamine

: 1116460-10-6
(S)-3-(4-(2-amino-6-chloropyrimidin-4-yl)phenyl)-2-(tert-butoxycarbonylamino)propanoic acid, tert-butylamine salt

Guidance literature:: In isopropyl alcohol; toluene; at 78 ℃; for 1h; Product distribution / selectivity;

Reference yield: 72.0%

: 1033804-86-2
(S)-3-[4-(2-amino-6-chloropyrimidin-4-yl)phenyl]-2-{[(tert-butoxy)carbonyl]amino}propanoic acid

: 75-64-9
tert-butylamine

: 1116460-10-6
(S)-3-(4-(2-amino-6-chloropyrimidin-4-yl)phenyl)-2-(tert-butoxycarbonylamino)propanoic acid, tert-butylamine salt

Guidance literature:: In isopropyl alcohol; toluene; at 0 - 78 ℃; for 2h; Product distribution / selectivity;

Reference yield:

: C₂₂H₂₃Cl₂N₇O₄

: 1125828-47-8
C₃₂H₃₉N₅O₈

: (S)-3-(4-(2-amino-6-chloropyrimidin-4-yl)phenyl)-2-(tert-butoxycarbonylamino)propanoic acid, potassium salt

: 75-64-9
tert-butylamine

: 1116460-10-6
(S)-3-(4-(2-amino-6-chloropyrimidin-4-yl)phenyl)-2-(tert-butoxycarbonylamino)propanoic acid, tert-butylamine salt

Guidance literature:: C₂₂H₂₃Cl₂N₇O₄; C₃₂H₃₉N₅O₈; (S)-3-(4-(2-amino-6-chloropyrimidin-4-yl)phenyl)-2-(tert-butoxycarbonylamino)propanoic acid, potassium salt; With hydrogenchloride; In tetrahydrofuran; water; toluene; at 60 ℃; pH=4.0;

tert-butylamine; In isopropyl alcohol; toluene; at 78 ℃; for 1h; Purification / work up;