[[4-[4-(aminosulfonyl)phenyl]-3-phenylisoxazol-5-yl]-methyloxy]acetic acid

Base Information

Chemical Name:[[4-[4-(aminosulfonyl)phenyl]-3-phenylisoxazol-5-yl]-methyloxy]acetic acid
CAS No.:181696-06-0
Molecular Formula:C₁₈H₁₆N₂O₆S
Molecular Weight:388.401
Hs Code.:

Synonyms:[[4-[4-(aminosulfonyl)phenyl]-3-phenylisoxazol-5-yl]-methyloxy]acetic acid

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Chemical Property of [[4-[4-(aminosulfonyl)phenyl]-3-phenylisoxazol-5-yl]-methyloxy]acetic acid

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Technology Process of [[4-[4-(aminosulfonyl)phenyl]-3-phenylisoxazol-5-yl]-methyloxy]acetic acid

There total 8 articles about [[4-[4-(aminosulfonyl)phenyl]-3-phenylisoxazol-5-yl]-methyloxy]acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 181697-09-6
[4-[4-[N-[2,5-dimethylpyrrol]sulfonyl]phenyl]-3-phenylisoxazol-5-yl]-methyloxyacetic acid

: 181696-06-0
[[4-[4-(aminosulfonyl)phenyl]-3-phenylisoxazol-5-yl]-methyloxy]acetic acid

Guidance literature:: With trifluoroacetic acid; In water; at 60 ℃; for 6h; Heating / reflux;

Reference yield:

: 181697-07-4
2-[4-[N-[2,5-dimethylpyrrol]-sulfonyl]phenyl]-1-phenyl-ethan-1-one oxime

: 181696-06-0
[[4-[4-(aminosulfonyl)phenyl]-3-phenylisoxazol-5-yl]-methyloxy]acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 1.17 h / -78 - 0 °C / Cooling with dry ice

1.2: 2 h / -78 - 20 °C

2.1: sulfuric acid / tetrahydrofuran / 1 h / Heating / reflux

3.1: trifluoroacetic acid / water / 6 h / 60 °C / Heating / reflux

With sulfuric acid; trifluoroacetic acid; lithium diisopropyl amide; In tetrahydrofuran; water;

Reference yield:

: 451-40-1
phenyl benzyl ketone

: 181696-06-0
[[4-[4-(aminosulfonyl)phenyl]-3-phenylisoxazol-5-yl]-methyloxy]acetic acid

Guidance literature:: Multi-step reaction with 7 steps

1.1: chlorosulfonic acid / 14 h / 5 - 20 °C

2.1: ammonia / water; acetone

3.1: thionyl chloride / ethanol / 0.5 h / Heating / reflux

4.1: hydroxylamine hydrochloride; sodium acetate / 14 h / Heating / reflux

5.1: lithium diisopropyl amide / tetrahydrofuran / 1.17 h / -78 - 0 °C / Cooling with dry ice

5.2: 2 h / -78 - 20 °C

6.1: sulfuric acid / tetrahydrofuran / 1 h / Heating / reflux

7.1: trifluoroacetic acid / water / 6 h / 60 °C / Heating / reflux

With chlorosulfonic acid; thionyl chloride; sulfuric acid; hydroxylamine hydrochloride; ammonia; sodium acetate; trifluoroacetic acid; lithium diisopropyl amide; In tetrahydrofuran; ethanol; water; acetone;