C₁₄H₁₃FO₂

Base Information

Chemical Name:C₁₄H₁₃FO₂
CAS No.:1304787-97-0
Molecular Formula:C₁₄H₁₃FO₂
Molecular Weight:232.254
Hs Code.:

C<sub>14</sub>H<sub>13</sub>FO<sub>2</sub>

Synonyms:C₁₄H₁₃FO₂

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Chemical Property of C₁₄H₁₃FO₂

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Technology Process of C₁₄H₁₃FO₂

There total 3 articles about C₁₄H₁₃FO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 18511-62-1,53631-23-5,134356-73-3,134356-74-4
(2S)-2-(4-fluorophenyl)oxirane

: 108-95-2,27073-41-2
phenol

: 1304787-97-0
C₁₄H₁₃FO₂

Guidance literature:: phenol; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.166667h; Inert atmosphere;

(2S)-2-(4-fluorophenyl)oxirane; In N,N-dimethyl-formamide; at 60 ℃; for 24h; optical yield given as %ee; Inert atmosphere;
DOI:10.1021/jo102294j

Reference yield:

: 1234372-12-3
(1S)-2-bromo-1-(4-fluorophenyl)ethan-1-ol

: 1304787-97-0
C₁₄H₁₃FO₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / tetrahydrofuran; water / 2 h

2.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 20 °C / Inert atmosphere

2.2: 24 h / 60 °C / Inert atmosphere

With sodium hydride; sodium hydroxide; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1021/jo102294j

Reference yield:

: 403-29-2
2-bromo-4'-fluoroacetophenone

: 1304787-97-0
C₁₄H₁₃FO₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: 2-[(1,3,2-dioxaborolan-2-yloxy)diphenylmethyl]pyrrolidine; dimethylsulfide borane complex / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

2.1: sodium hydroxide / tetrahydrofuran; water / 2 h

3.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 20 °C / Inert atmosphere

3.2: 24 h / 60 °C / Inert atmosphere

With 2-[(1,3,2-dioxaborolan-2-yloxy)diphenylmethyl]pyrrolidine; dimethylsulfide borane complex; sodium hydride; sodium hydroxide; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1021/jo102294j