(1-(1-benzoylcyclopropanecarbonyl)cyclopropyl)(4-tert-butylphenyl)methanone

Base Information

Chemical Name:(1-(1-benzoylcyclopropanecarbonyl)cyclopropyl)(4-tert-butylphenyl)methanone
CAS No.:1318801-10-3
Molecular Formula:C₂₅H₂₆O₃
Molecular Weight:374.48
Hs Code.:

Synonyms:(1-(1-benzoylcyclopropanecarbonyl)cyclopropyl)(4-tert-butylphenyl)methanone

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Chemical Property of (1-(1-benzoylcyclopropanecarbonyl)cyclopropyl)(4-tert-butylphenyl)methanone

Chemical Property:

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Technology Process of (1-(1-benzoylcyclopropanecarbonyl)cyclopropyl)(4-tert-butylphenyl)methanone

There total 3 articles about (1-(1-benzoylcyclopropanecarbonyl)cyclopropyl)(4-tert-butylphenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: C₂₃H₂₄O₃

: 106-93-4
ethylene dibromide

: 1318801-10-3
(1-(1-benzoylcyclopropanecarbonyl)cyclopropyl)(4-tert-butylphenyl)methanone

Guidance literature:: With potassium carbonate; In dimethyl sulfoxide; at 20 ℃;
DOI:10.1039/c1ob05455d

Reference yield:

: 93-91-4
1-phenylbutan-1,3-dione

: 1318801-10-3
(1-(1-benzoylcyclopropanecarbonyl)cyclopropyl)(4-tert-butylphenyl)methanone

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / dimethyl sulfoxide / 20 °C

2.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C

2.2: -78 - 20 °C

3.1: potassium carbonate / dimethyl sulfoxide / 20 °C

With potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; dimethyl sulfoxide; 2.1: Claisen condensation / 2.2: Claisen condensation;
DOI:10.1039/c1ob05455d

Reference yield:

: 5186-09-4
1-acetyl-1-benzoyl cyclopropane

: 1318801-10-3
(1-(1-benzoylcyclopropanecarbonyl)cyclopropyl)(4-tert-butylphenyl)methanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C

1.2: -78 - 20 °C

2.1: potassium carbonate / dimethyl sulfoxide / 20 °C

With potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; dimethyl sulfoxide; 1.1: Claisen condensation / 1.2: Claisen condensation;
DOI:10.1039/c1ob05455d