diethyl 4-(3,4,5-trimethoxylphenyl)-1,4-dihydropyridine-3,5-dicarboxylate

Base Information

Chemical Name:diethyl 4-(3,4,5-trimethoxylphenyl)-1,4-dihydropyridine-3,5-dicarboxylate
CAS No.:120533-65-5
Molecular Formula:C₂₀H₂₅NO₇
Molecular Weight:391.421
Hs Code.:

Synonyms:diethyl 4-(3,4,5-trimethoxylphenyl)-1,4-dihydropyridine-3,5-dicarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl 4-(3,4,5-trimethoxylphenyl)-1,4-dihydropyridine-3,5-dicarboxylate

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Technology Process of diethyl 4-(3,4,5-trimethoxylphenyl)-1,4-dihydropyridine-3,5-dicarboxylate

There total 1 articles about diethyl 4-(3,4,5-trimethoxylphenyl)-1,4-dihydropyridine-3,5-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 623-47-2
propynoic acid ethyl ester

: 120533-65-5
diethyl 4-(3,4,5-trimethoxylphenyl)-1,4-dihydropyridine-3,5-dicarboxylate

Guidance literature:: With ammonium acetate; acetic acid; In ethanol; Microwave irradiation; Heating;
DOI:10.1039/c8nj02192a

Reference yield: 86.0%

: 120533-65-5
diethyl 4-(3,4,5-trimethoxylphenyl)-1,4-dihydropyridine-3,5-dicarboxylate

: 88-95-9
Phthaloyl dichloride

: tetraethyl 1,1'-phthaloylbis(4-(3,4,5-trimethoxyphenyl)-1,4-dihydropyridine-3,5-dicarboxylate)

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1016/j.tet.2017.10.019

Reference yield: 81.0%

: 120533-65-5
diethyl 4-(3,4,5-trimethoxylphenyl)-1,4-dihydropyridine-3,5-dicarboxylate

: 17465-86-0
cyclomaltooctaose

: 2C₄₈H₈₀O₄₀*C₄₀H₅₀N₂O₁₄

Guidance literature:: In tetrahydrofuran; water; at 60 ℃; for 10h; stereoselective reaction; Inert atmosphere; Sonication; Irradiation;
DOI:10.1016/j.jphotochem.2018.03.046