2-(2-methoxyphenyl)propen-2-oyl chloride

Base Information

Chemical Name:2-(2-methoxyphenyl)propen-2-oyl chloride
CAS No.:349552-88-1
Molecular Formula:C₁₀H₉ClO₂
Molecular Weight:196.633
Hs Code.:

Synonyms:2-(2-methoxyphenyl)propen-2-oyl chloride

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Chemical Property of 2-(2-methoxyphenyl)propen-2-oyl chloride

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Technology Process of 2-(2-methoxyphenyl)propen-2-oyl chloride

There total 4 articles about 2-(2-methoxyphenyl)propen-2-oyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 81616-75-3
2-methoxy-α-methylene-benzeneacetic acid

: 349552-88-1
2-(2-methoxyphenyl)propen-2-oyl chloride

Guidance literature:: With thionyl chloride; In dichloromethane; at 20 ℃; for 15h;
DOI:10.1021/jo0100188

Reference yield:

: 93-25-4
2-methoxyphenylacetic acid

: 349552-88-1
2-(2-methoxyphenyl)propen-2-oyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid / 3 h / Reflux

2: potassium carbonate; tetra(n-butyl)ammonium hydrogensulfate / toluene / 12 h / 80 °C

3: lithium hydroxide monohydrate / tetrahydrofuran; water / 3 h / Heating

4: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3 h / 0 - 20 °C

With oxalyl dichloride; lithium hydroxide monohydrate; sulfuric acid; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; water; toluene;
DOI:10.1002/anie.201710601

Reference yield:

: 27798-60-3
methyl 2-(2-methoxyphenyl)acetate

: 349552-88-1
2-(2-methoxyphenyl)propen-2-oyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; tetra(n-butyl)ammonium hydrogensulfate / toluene / 12 h / 80 °C

2: lithium hydroxide monohydrate / tetrahydrofuran; water / 3 h / Heating

3: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3 h / 0 - 20 °C

With oxalyl dichloride; lithium hydroxide monohydrate; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; water; toluene;
DOI:10.1002/anie.201710601