Technology Process of C26H22N6O4S
There total 7 articles about C26H22N6O4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
acetonitrile;
at 100 ℃;
for 0.5h;
Microwaves;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 20 °C
1.2: 18 h / 0 - 20 °C
2.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate / 1,4-dioxane; water / 1 h / 60 °C
3.1: trimethylsilylazide; dibutyl(oxo)stannane / toluene / 23.75 h / -120 - 20 °C
4.1: chloroform / 0.5 h / 100 °C / Microwave irradiation
5.1: hydrogenchloride; ammonia / acetonitrile / 0.5 h / 100 °C / Microwave irradiation
With
hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; trimethylsilylazide; ammonia; sodium hydride; dibutyl(oxo)stannane;
In
1,4-dioxane; chloroform; water; N,N-dimethyl-formamide; toluene; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 20 °C
1.2: 18 h / 0 - 20 °C
2.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate / 1,4-dioxane; water / 1 h / 60 °C
3.1: trimethylsilylazide; dibutyl(oxo)stannane / toluene / 23.75 h / -120 - 20 °C
4.1: chloroform / 0.5 h / 100 °C / Microwave irradiation
5.1: hydrogenchloride; ammonia / acetonitrile / 0.5 h / 100 °C / Microwave irradiation
With
hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; trimethylsilylazide; ammonia; sodium hydride; dibutyl(oxo)stannane;
In
1,4-dioxane; chloroform; water; N,N-dimethyl-formamide; toluene; acetonitrile;