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C19H23F2NO

Base Information
  • Chemical Name:C19H23F2NO
  • CAS No.:1412899-21-8
  • Molecular Formula:C19H23F2NO
  • Molecular Weight:319.395
  • Hs Code.:
C<sub>19</sub>H<sub>23</sub>F<sub>2</sub>NO

Synonyms:C19H23F2NO

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Chemical Property of C19H23F2NO
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Technology Process of C19H23F2NO

There total 1 articles about C19H23F2NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
formic acid; With acetic anhydride; at 60 ℃; for 5h;
C18H21F2NO; at 20 ℃; for 0.5h;
With dimethylsulfide borane complex; In tetrahydrofuran; at 0 ℃; for 2h; Reflux;
DOI:10.1021/ja310209g
Guidance literature:
C19H23F2NO; With hydrogenchloride; In methanol;
With sodium azide; trifluorormethanesulfonic acid; trifluoroacetic acid; at 0 ℃; for 2h;
DOI:10.1021/ja310209g
Guidance literature:
Multi-step reaction with 4 steps
1.1: hydrogenchloride / methanol
1.2: 2 h / 0 °C
2.1: ammonium formate; zinc / methanol / 1 h / 20 °C
3.1: triethylamine; phosphorus trichloride / toluene / 16 h
4.1: Amberlyst A-26 OH form / methanol
With hydrogenchloride; ammonium formate; triethylamine; zinc; phosphorus trichloride; In methanol; toluene;
DOI:10.1021/ja310209g
upstream raw materials:

formic acid

C18H21F2NO

Downstream raw materials:

C38H43F4N4P

C19H24F2N2

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