1,3,4,6-tetrakis[(acetyloxy)methyl]tetrahydro-3a,6a-diphenyl-imidazo[4,5-d]imidazole-2,5(1H,3H)-dione

Base Information

Chemical Name:1,3,4,6-tetrakis[(acetyloxy)methyl]tetrahydro-3a,6a-diphenyl-imidazo[4,5-d]imidazole-2,5(1H,3H)-dione
CAS No.:1352409-24-5
Molecular Formula:C₂₈H₃₀N₄O₁₀
Molecular Weight:582.567
Hs Code.:

Synonyms:1,3,4,6-tetrakis[(acetyloxy)methyl]tetrahydro-3a,6a-diphenyl-imidazo[4,5-d]imidazole-2,5(1H,3H)-dione

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Chemical Property of 1,3,4,6-tetrakis[(acetyloxy)methyl]tetrahydro-3a,6a-diphenyl-imidazo[4,5-d]imidazole-2,5(1H,3H)-dione

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Technology Process of 1,3,4,6-tetrakis[(acetyloxy)methyl]tetrahydro-3a,6a-diphenyl-imidazo[4,5-d]imidazole-2,5(1H,3H)-dione

There total 3 articles about 1,3,4,6-tetrakis[(acetyloxy)methyl]tetrahydro-3a,6a-diphenyl-imidazo[4,5-d]imidazole-2,5(1H,3H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 108-24-7
acetic anhydride

: 111380-75-7
1,3,4,6-bis(2-oxapropylene)tetrahydro-3a,6a-diphenylimidazo<4,5-d>imidazole-2,5(1H,3H)-dione

: 1352409-24-5
1,3,4,6-tetrakis[(acetyloxy)methyl]tetrahydro-3a,6a-diphenyl-imidazo[4,5-d]imidazole-2,5(1H,3H)-dione

Guidance literature:: With toluene-4-sulfonic acid; at 110 ℃; for 3h;
DOI:10.1039/c1cc15125h

Reference yield:

: 101241-21-8
3a,6a-diphenylglycoluril

: 1352409-24-5
1,3,4,6-tetrakis[(acetyloxy)methyl]tetrahydro-3a,6a-diphenyl-imidazo[4,5-d]imidazole-2,5(1H,3H)-dione

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / dimethyl sulfoxide / 20 °C / pH 9

1.2: 2 h / 100 °C / pH 1

2.1: toluene-4-sulfonic acid / 3 h / 110 °C

With toluene-4-sulfonic acid; sodium hydroxide; In dimethyl sulfoxide;
DOI:10.1039/c1cc15125h

Reference yield:

: 134-81-6
benzil

: 1352409-24-5
1,3,4,6-tetrakis[(acetyloxy)methyl]tetrahydro-3a,6a-diphenyl-imidazo[4,5-d]imidazole-2,5(1H,3H)-dione

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoroacetic acid / toluene / Reflux

2.1: sodium hydroxide / dimethyl sulfoxide / 20 °C / pH 9

2.2: 2 h / 100 °C / pH 1

3.1: toluene-4-sulfonic acid / 3 h / 110 °C

With toluene-4-sulfonic acid; trifluoroacetic acid; sodium hydroxide; In dimethyl sulfoxide; toluene;
DOI:10.1039/c1cc15125h