N-(6-acetyl-2-chloro-3-methoxyphenyl)-5-isopropylisoxazole-3-carboxamide

Base Information

Chemical Name:N-(6-acetyl-2-chloro-3-methoxyphenyl)-5-isopropylisoxazole-3-carboxamide
CAS No.:1180495-62-8
Molecular Formula:C₁₆H₁₇ClN₂O₄
Molecular Weight:336.775
Hs Code.:

Synonyms:N-(6-acetyl-2-chloro-3-methoxyphenyl)-5-isopropylisoxazole-3-carboxamide

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Chemical Property of N-(6-acetyl-2-chloro-3-methoxyphenyl)-5-isopropylisoxazole-3-carboxamide

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Technology Process of N-(6-acetyl-2-chloro-3-methoxyphenyl)-5-isopropylisoxazole-3-carboxamide

There total 3 articles about N-(6-acetyl-2-chloro-3-methoxyphenyl)-5-isopropylisoxazole-3-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 89776-74-9
5-isopropylisoxazole-3-carboxylic acid

: 79-37-8
oxalyl dichloride

: 923289-36-5
1-(2-amino-3-chloro-4-methoxy-phenyl)ethanone

: 1180495-62-8
N-(6-acetyl-2-chloro-3-methoxyphenyl)-5-isopropylisoxazole-3-carboxamide

Guidance literature:: With sodium hydrogencarbonate; In 1,4-dioxane; diethyl ether; 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran;

Reference yield:

: 53064-56-5
C₇H₈ClNO₂

: 923289-36-5
1-(2-amino-3-chloro-4-methoxy-phenyl)ethanone

: 1180495-62-8
N-(6-acetyl-2-chloro-3-methoxyphenyl)-5-isopropylisoxazole-3-carboxamide

Guidance literature:: C₇H₈ClNO₂; 1-(2-amino-3-chloro-4-methoxy-phenyl)ethanone; In 1,4-dioxane; at 20 ℃; for 16h; Inert atmosphere;

With sodium hydrogencarbonate; In 1,4-dioxane;

Reference yield:

: 89776-74-9
5-isopropylisoxazole-3-carboxylic acid

: 1180495-62-8
N-(6-acetyl-2-chloro-3-methoxyphenyl)-5-isopropylisoxazole-3-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

2: 1,4-dioxane / 16 h / 20 °C / Inert atmosphere

With oxalyl dichloride; N,N-dimethyl-formamide; In 1,4-dioxane; dichloromethane;