Methyl 1-(N-benzyloxycarbonyl-N-methyl)aminocyclopropane-1-carboxylic acid

Base Information

Chemical Name:Methyl 1-(N-benzyloxycarbonyl-N-methyl)aminocyclopropane-1-carboxylic acid
CAS No.:210576-30-0
Molecular Formula:C₁₄H₁₇NO₄
Molecular Weight:263.293
Hs Code.:

Synonyms:Methyl 1-(N-benzyloxycarbonyl-N-methyl)aminocyclopropane-1-carboxylic acid

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Chemical Property of Methyl 1-(N-benzyloxycarbonyl-N-methyl)aminocyclopropane-1-carboxylic acid

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Technology Process of Methyl 1-(N-benzyloxycarbonyl-N-methyl)aminocyclopropane-1-carboxylic acid

There total 2 articles about Methyl 1-(N-benzyloxycarbonyl-N-methyl)aminocyclopropane-1-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 84677-05-4
methyl 1-(((benzyloxy)carbonyl)amino)cyclopropane-1-carboxylate

: 74-88-4
methyl iodide

: 210576-30-0
Methyl 1-(N-benzyloxycarbonyl-N-methyl)aminocyclopropane-1-carboxylic acid

Guidance literature:: With silver(l) oxide; In N,N-dimethyl-formamide; at 50 - 60 ℃; for 96h;
DOI:10.1016/S0014-827X(98)00005-6

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 210576-30-0
Methyl 1-(N-benzyloxycarbonyl-N-methyl)aminocyclopropane-1-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / NaHCO₃, H₂O / Ambient temperature

2: 38 percent / Ag₂O / dimethylformamide / 96 h / 50 - 60 °C

With water; sodium hydrogencarbonate; silver(l) oxide; In N,N-dimethyl-formamide;
DOI:10.1016/S0014-827X(98)00005-6

Reference yield:

: 210576-30-0
Methyl 1-(N-benzyloxycarbonyl-N-methyl)aminocyclopropane-1-carboxylic acid

: 119111-66-9
1-methylamino-cyclopropanecarboxylic acid methyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 1.5h; under 1140 Torr; Ambient temperature;
DOI:10.1016/S0014-827X(98)00005-6