SiF₃SiHBr₂

Base Information

Chemical Name:SiF₃SiHBr₂
CAS No.:56144-86-6
Molecular Formula:Br₂F₃HSi₂
Molecular Weight:273.982
Hs Code.:

Synonyms:SiF₃SiHBr₂

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Chemical Property of SiF₃SiHBr₂

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Technology Process of SiF₃SiHBr₂

There total 1 articles about SiF₃SiHBr₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 56144-87-7
SiF₃SiFHBr

: 1631-73-8
trimethylstannane

: 24628-33-9
SiF₃SiF₂H

: 56144-86-6
SiF₃SiHBr₂

: 15195-26-3
F₃SiSiH₃

: 1066-44-0
trimethyltin bromide

Guidance literature:: In neat (no solvent); Warming mixt. of equimolar amt. of starting materials (condensed at -196°C) to -80°C (30 min) and then gradually to 10°C.; Removal of Me3SnCl by passing the mixt. through a trap cooled to -95°C (toluene). NMR spectrum indicate presence of major resulting compounds, with small amt. of SiF3SiHBr2 and unreacted SiF3SiFHBr.;

Reference yield: 90.0%

: 56144-86-6
SiF₃SiHBr₂

: 1631-73-8
trimethylstannane

: 15195-26-3
F₃SiSiH₃

: 1066-44-0
trimethyltin bromide

Guidance literature:: In neat (no solvent); Warming of starting materials (in absence of solvent, vac. line) for 30 min to room temp.; Removal of Me3SnBr by passing the mixt. through a trap cooled to -95°C (toluene), IR and NMR identification of volatile resulting compd.;

Reference yield: 45.0%

: 16853-85-3
lithium aluminium tetrahydride

: 56144-86-6
SiF₃SiHBr₂

: 1590-87-0
disilane

: 13465-71-9
trifluorosilane

: 7783-61-1
silicon tetrafluoride

Guidance literature:: React. occurs at room temp. (N2 or Ar, 15 min).; IR spectrum of volatile material indicates resulting compounds and 5% unreacted SiF3SiHBr2.;

upstream raw materials:

SiF₃SiFHBr

trimethylstannane

Downstream raw materials:

disilane

trifluorosilane

silicon tetrafluoride

monosilane

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