methyl (2S,3R)-N-(p-toluenesulfonyl)-3-amino-3-phenyl-2-hydroxypropanoate

Base Information

Chemical Name:methyl (2S,3R)-N-(p-toluenesulfonyl)-3-amino-3-phenyl-2-hydroxypropanoate
CAS No.:58107-45-2
Molecular Formula:C₁₇H₁₉NO₅S
Molecular Weight:349.408
Hs Code.:

Synonyms:methyl (2S,3R)-N-(p-toluenesulfonyl)-3-amino-3-phenyl-2-hydroxypropanoate

Suppliers and Price of methyl (2S,3R)-N-(p-toluenesulfonyl)-3-amino-3-phenyl-2-hydroxypropanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (2S,3R)-N-(p-toluenesulfonyl)-3-amino-3-phenyl-2-hydroxypropanoate

Chemical Property:

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Technology Process of methyl (2S,3R)-N-(p-toluenesulfonyl)-3-amino-3-phenyl-2-hydroxypropanoate

There total 6 articles about methyl (2S,3R)-N-(p-toluenesulfonyl)-3-amino-3-phenyl-2-hydroxypropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 127-65-1
chloroamine-T

: 103-26-4,1754-62-7
Methyl cinnamate

: 58107-45-2
methyl (2S,3R)-N-(p-toluenesulfonyl)-3-amino-3-phenyl-2-hydroxypropanoate

: 176298-46-7
2-hydroxy-3-(4-methyl benzenesulfonylamino)-3-phenyl-propionic acid methyl ester

Guidance literature:: With potassium dioxotetrahydroxoosmate(VI); (DHQ)2-PHAL; In water; tert-butyl alcohol; Title compound not separated from byproducts; Ambient temperature;
DOI:10.3891/acta.chem.scand.50-0649

Reference yield:

: 825627-66-5
methyl (3R)-2-oxo-3-phenyl-3-[(N-tosyl)amino]propanoate

: 58107-45-2
methyl (2S,3R)-N-(p-toluenesulfonyl)-3-amino-3-phenyl-2-hydroxypropanoate

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 24h; under 760 Torr;
DOI:10.1002/anie.200460730

Reference yield:

: 825627-55-2
methyl (3R)-2-diazo-3-phenyl-3-[(N-tosyl)amino]propanoate

: 58107-45-2
methyl (2S,3R)-N-(p-toluenesulfonyl)-3-amino-3-phenyl-2-hydroxypropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: dimethyldioxirane / acetone / 5 h / 0 °C

2: H₂ / Pd/C / methanol / 24 h / 20 °C / 760 Torr

With hydrogen; 3,3-dimethyldioxirane; palladium on activated charcoal; In methanol; acetone;
DOI:10.1002/anie.200460730