thiocarbonic acid O-{4-[4-(1-benzyloxy-hexyl)-phenyl]-2-oxo-hexahydro-cyclopenta[b]furan-5-yl} ester O-phenyl ester

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Chemical Name:thiocarbonic acid O-{4-[4-(1-benzyloxy-hexyl)-phenyl]-2-oxo-hexahydro-cyclopenta[b]furan-5-yl} ester O-phenyl ester
CAS No.:879098-90-5
Molecular Formula:C₃₃H₃₆O₅S
Molecular Weight:544.712
Hs Code.:

thiocarbonic acid <i>O</i>-{4-[4-(1-benzyloxy-hexyl)-phenyl]-2-oxo-hexahydro-cyclopenta[<i>b</i>]furan-5-yl} ester <i>O</i>-phenyl ester

Synonyms:thiocarbonic acid O-{4-[4-(1-benzyloxy-hexyl)-phenyl]-2-oxo-hexahydro-cyclopenta[b]furan-5-yl} ester O-phenyl ester

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Chemical Property of thiocarbonic acid O-{4-[4-(1-benzyloxy-hexyl)-phenyl]-2-oxo-hexahydro-cyclopenta[b]furan-5-yl} ester O-phenyl ester

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Technology Process of thiocarbonic acid O-{4-[4-(1-benzyloxy-hexyl)-phenyl]-2-oxo-hexahydro-cyclopenta[b]furan-5-yl} ester O-phenyl ester

There total 5 articles about thiocarbonic acid O-{4-[4-(1-benzyloxy-hexyl)-phenyl]-2-oxo-hexahydro-cyclopenta[b]furan-5-yl} ester O-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 879098-89-2
(3aR,4S,5R,6aS)-4-[4-(1-Benzyloxy-hexyl)-phenyl]-5-hydroxy-hexahydro-cyclopenta[b]furan-2-one

: 1005-56-7
phenylcarbonochloridothioate

: 879098-90-5
thiocarbonic acid O-{4-[4-(1-benzyloxy-hexyl)-phenyl]-2-oxo-hexahydro-cyclopenta[b]furan-5-yl} ester O-phenyl ester

Guidance literature:: With pyridine; dmap; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1021/ja057560o

Reference yield:

: 879098-65-4
Acetic acid (1R,4S)-4-(1-butoxy-2-iodo-ethoxy)-cyclopent-2-enyl ester

: 879098-90-5
thiocarbonic acid O-{4-[4-(1-benzyloxy-hexyl)-phenyl]-2-oxo-hexahydro-cyclopenta[b]furan-5-yl} ester O-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: CoCl₂; (R,R)-1,2-bis(dimethylamino)cyclohexane / tetrahydrofuran / 0.25 h / 25 °C

1.2: 54 percent / Jones reagent / acetone / 20 °C

2.1: 85 percent / K₂CO₃ / methanol / 0.5 h / 20 °C

3.1: pyridine; N,N-dimethyl-4-aminopyridine / CH₂Cl₂ / 12 h / 20 °C

With pyridine; dmap; (1R,2R)-bis(dimethylamino)cyclohexane; potassium carbonate; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ja057560o

Reference yield:

: C₁₉H₂₃BrMgO

: 879098-90-5
thiocarbonic acid O-{4-[4-(1-benzyloxy-hexyl)-phenyl]-2-oxo-hexahydro-cyclopenta[b]furan-5-yl} ester O-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: CoCl₂; (R,R)-1,2-bis(dimethylamino)cyclohexane / tetrahydrofuran / 0.25 h / 25 °C

1.2: 54 percent / Jones reagent / acetone / 20 °C

2.1: 85 percent / K₂CO₃ / methanol / 0.5 h / 20 °C

3.1: pyridine; N,N-dimethyl-4-aminopyridine / CH₂Cl₂ / 12 h / 20 °C

With pyridine; dmap; (1R,2R)-bis(dimethylamino)cyclohexane; potassium carbonate; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ja057560o