Thiol-dPEG5-azido

Base Information

Chemical Name:Thiol-dPEG5-azido
CAS No.:1347750-79-1
Molecular Formula:C₈H₁₇N₃O₃S
Molecular Weight:235.307
Hs Code.:
Mol file:1347750-79-1.mol

Synonyms:2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethanethiol

Suppliers and Price of Thiol-dPEG5-azido

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

purepeg
HS-PEG3-CH2CH2N3 min.95%
250 mg
$ 400.00

purepeg
HS-PEG3-CH2CH2N3 min.95%
1 g
$ 675.00

ChemPep
N3-CH2CH2-PEG3-SH
1g
$ 592.00

ChemPep
N3-CH2CH2-PEG3-SH
500mg
$ 385.00

Total 7 raw suppliers

Chemical Property of Thiol-dPEG5-azido

Chemical Property:

Purity/Quality:

98%,99%, ^*data from raw suppliers

HS-PEG3-CH2CH2N3 min.95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Thiol-dPEG5-azido

There total 4 articles about Thiol-dPEG5-azido which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1310827-26-9
S-2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethyl ethanethioate

: 1347750-79-1
2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethanethiol

Guidance literature:: With hydrogenchloride; sodium hydroxide; In methanol; ethanol; water; for 0.916667h; Inert atmosphere;
DOI:10.1039/c3cc41634h

Reference yield:

: 168640-82-2
11-azido-3,6,9-trioxa-undecanyl p-toluenesulfonate

: 1347750-79-1
2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethanethiol

Guidance literature:: Multi-step reaction with 2 steps

1: acetone / 50 °C

2: sodium hydroxide; hydrogenchloride / methanol; ethanol; water / 0.92 h / Inert atmosphere

With hydrogenchloride; sodium hydroxide; In methanol; ethanol; water; acetone;
DOI:10.1039/c3cc41634h

Reference yield:

: 37860-51-8
tetraethylene glycol di(p-toluenesulfonate)

: 1347750-79-1
2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethanethiol

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide / acetonitrile / Reflux

2: acetone / 50 °C

3: sodium hydroxide; hydrogenchloride / methanol; ethanol; water / 0.92 h / Inert atmosphere

With hydrogenchloride; sodium azide; sodium hydroxide; In methanol; ethanol; water; acetone; acetonitrile;
DOI:10.1039/c3cc41634h