4,5,6,7,8,9,10,11,12,13-decahydro-2,3-diphenylcyclododeca[b]furan

Base Information

• Chemical Name: 4,5,6,7,8,9,10,11,12,13-decahydro-2,3-diphenylcyclododeca[b]furan
• CAS No.: 1032196-79-4
• Molecular Formula: C₂₆H₃₀O
• Molecular Weight: 358.524
• Mol file: 1032196-79-4.mol

Synonyms:4,5,6,7,8,9,10,11,12,13-decahydro-2,3-diphenylcyclododeca[b]furan

Chemical Property of 4,5,6,7,8,9,10,11,12,13-decahydro-2,3-diphenylcyclododeca[b]furan

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4,5,6,7,8,9,10,11,12,13-decahydro-2,3-diphenylcyclododeca[b]furan

There total 1 articles about 4,5,6,7,8,9,10,11,12,13-decahydro-2,3-diphenylcyclododeca[b]furan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

4,5,6,7,8,9,10,11,12,13-decahydro-3-iodo-2-phenylcyclododeca[b]furan (1032196-70-5) + phenylboronic acid (98-80-6) → 4,5,6,7,8,9,10,11,12,13-decahydro-2,3-diphenylcyclododeca[b]furan (1032196-79-4)

Guidance literature:

With palladium diacetate; potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 6h;

DOI:10.1002/ejoc.200700963

Reference yield:

methanol (67-56-1) + 4,5,6,7,8,9,10,11,12,13-decahydro-2,3-diphenylcyclododeca[b]furan (1032196-79-4) → C27H34O4

Guidance literature:

With oxygen; methylene blue; In Petroleum ether; at 0 ℃; for 0.5h; Irradiation;

DOI:10.1002/ejoc.201901613

Reference yield:

4,5,6,7,8,9,10,11,12,13-decahydro-2,3-diphenylcyclododeca[b]furan (1032196-79-4) → C27H32O3

Guidance literature:

Multi-step reaction with 2 steps

1: oxygen; methylene blue / Petroleum ether / 0.5 h / 0 °C / Irradiation

2: iron(II) lactate; copper diacetate / water; dimethyl sulfoxide / 0.5 h / 20 °C

With iron(II) lactate; oxygen; copper diacetate; methylene blue; In water; dimethyl sulfoxide; Petroleum ether;

DOI:10.1002/ejoc.201901613

upstream raw materials:

4,5,6,7,8,9,10,11,12,13-decahydro-3-iodo-2-phenylcyclododeca[b]furan

phenylboronic acid