(4R,6R)-4-(2-Benzyloxy-ethyl)-2,2-dimethyl-6-oxiranylmethyl-[1,3]dioxane

Base Information

Chemical Name:(4R,6R)-4-(2-Benzyloxy-ethyl)-2,2-dimethyl-6-oxiranylmethyl-[1,3]dioxane
CAS No.:853923-32-7
Molecular Formula:C₁₈H₂₆O₄
Molecular Weight:306.402
Hs Code.:

Synonyms:(4R,6R)-4-(2-Benzyloxy-ethyl)-2,2-dimethyl-6-oxiranylmethyl-[1,3]dioxane

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Chemical Property of (4R,6R)-4-(2-Benzyloxy-ethyl)-2,2-dimethyl-6-oxiranylmethyl-[1,3]dioxane

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Technology Process of (4R,6R)-4-(2-Benzyloxy-ethyl)-2,2-dimethyl-6-oxiranylmethyl-[1,3]dioxane

There total 13 articles about (4R,6R)-4-(2-Benzyloxy-ethyl)-2,2-dimethyl-6-oxiranylmethyl-[1,3]dioxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 853923-24-7
(4S,6S)-4-[2-(benzyloxy)ethyl]-2,2-dimethyl-6-(prop-2-en-1-yl)-1,3-dioxane

: 853923-32-7
(4R,6R)-4-(2-Benzyloxy-ethyl)-2,2-dimethyl-6-oxiranylmethyl-[1,3]dioxane

: 3-[(4S,6R)-6-(2-Benzyloxy-ethyl)-2,2-dimethyl-[1,3]dioxan-4-yl]-propane-1,2-diol

Guidance literature:: (4S,6S)-4-[2-(benzyloxy)ethyl]-2,2-dimethyl-6-(prop-2-en-1-yl)-1,3-dioxane; With Oxone; ethylenediaminetetraacetic acid; sodium hydrogencarbonate; In acetone;

With (R,R)-(salen)Co(III)(OAc); water;
DOI:10.1016/j.tetlet.2005.03.202

Reference yield:

: Benzoic acid 3-[(4R,6R)-6-(2-benzyloxy-ethyl)-2,2-dimethyl-[1,3]dioxan-4-yl]-2-(toluene-4-sulfonyloxy)-propyl ester

: 853923-32-7
(4R,6R)-4-(2-Benzyloxy-ethyl)-2,2-dimethyl-6-oxiranylmethyl-[1,3]dioxane

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃;
DOI:10.1016/j.tetlet.2005.03.202

Reference yield:

: 853923-30-5
(3R,5S)-1-(benzyloxy)oct-7-ene-3,5-diol

: 853923-32-7
(4R,6R)-4-(2-Benzyloxy-ethyl)-2,2-dimethyl-6-oxiranylmethyl-[1,3]dioxane

Guidance literature:: Multi-step reaction with 2 steps

1.1: 94 percent / PTSA / dimethylsulfoxide

2.1: oxone; NaHCO₃; EDTA / acetone

2.2: 43 percent / H₂O; (R,R)-(salen)Co(III)(OAc)

With Oxone; ethylenediaminetetraacetic acid; sodium hydrogencarbonate; toluene-4-sulfonic acid; In dimethyl sulfoxide; acetone;
DOI:10.1016/j.tetlet.2005.03.202