methyl trifluoroacetylurethane

Base Information

• Chemical Name: methyl trifluoroacetylurethane
• CAS No.: 146463-86-7
• Molecular Formula: C₄H₄F₃NO₃
• Molecular Weight: 171.076
• Mol file: 146463-86-7.mol

Synonyms:methyl trifluoroacetylurethane

Chemical Property of methyl trifluoroacetylurethane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl trifluoroacetylurethane

There total 2 articles about methyl trifluoroacetylurethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diisopropylcyanamide (3085-76-5) + trifluoroacetic anhydride (407-25-0) → N,N-diisopropylurea (77464-05-2) + trifluoroacetic acid-methyl ester (431-47-0) + methyl trifluoroacetylurethane (146463-86-7)

Guidance literature:

With methanol; Yield given. Multistep reaction. Yields of byproduct given; 1.) Et₂O, -20 deg C to 25 deg C, 2.) C₆D₆;

DOI:10.1021/jo9710184

Reference yield:

methanol (67-56-1) + diisopropylcyanamide (3085-76-5) + trifluoroacetic anhydride (407-25-0) → N,N-diisopropylurea (77464-05-2) + trifluoroacetic acid-methyl ester (431-47-0) + methyl trifluoroacetylurethane (146463-86-7)

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given; 1.) Et₂O, -20 deg C to 25 deg C, 2.) C₆D₆;

DOI:10.1021/jo9710184

upstream raw materials:

methanol

diisopropylcyanamide

trifluoroacetic anhydride