N-<6-(2,6-dichlorophenyl)-2-methylpyrido<2,3-d>pyrimidin-7-yl>-N'-methylthiourea

Base Information

• Chemical Name: N-<6-(2,6-dichlorophenyl)-2-methylpyrido<2,3-d>pyrimidin-7-yl>-N'-methylthiourea
• CAS No.: 77206-77-0
• Molecular Formula: C₁₆H₁₃Cl₂N₅S
• Molecular Weight: 378.285

Synonyms:N-<6-(2,6-dichlorophenyl)-2-methylpyrido<2,3-d>pyrimidin-7-yl>-N'-methylthiourea

Chemical Property of N-<6-(2,6-dichlorophenyl)-2-methylpyrido<2,3-d>pyrimidin-7-yl>-N'-methylthiourea

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Technology Process of N-<6-(2,6-dichlorophenyl)-2-methylpyrido<2,3-d>pyrimidin-7-yl>-N'-methylthiourea

There total 1 articles about N-<6-(2,6-dichlorophenyl)-2-methylpyrido<2,3-d>pyrimidin-7-yl>-N'-methylthiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-(2,6-dichlorophenyl)-2-methylpyrido<2,3-d>pyrimidin-7-amine (76574-80-6) + methyl thioisocyanate (556-61-6) → N-<6-(2,6-dichlorophenyl)-2-methylpyrido<2,3-d>pyrimidin-7-yl>-N'-methylthiourea (77206-77-0)

Guidance literature:

In toluene; for 30h; Heating;

DOI:10.1021/jm00357a015

Reference yield: 29.0%

N-<6-(2,6-dichlorophenyl)-2-methylpyrido<2,3-d>pyrimidin-7-yl>-N'-methylthiourea (77206-77-0) + methylamine (74-89-5) → N-[6-(2,6-Dichloro-phenyl)-2-methyl-pyrido[2,3-d]pyrimidin-7-yl]-N',N''-dimethyl-guanidine (77206-79-2)

Guidance literature:

With mercury(II) oxide; In ethanol; for 0.333333h; Heating;

DOI:10.1021/jm00357a015

Reference yield:

mercury(II) oxide (21908-53-2,12653-71-3) + N-<6-(2,6-dichlorophenyl)-2-methylpyrido<2,3-d>pyrimidin-7-yl>-N'-methylthiourea (77206-77-0) → N-[6-(2,6-dichlorophenyl)-2-methylyrido[2,3-d]pyrimidin-7-yl]-N',N-dimethylguanidine + N-[6-(2,6-dichlorophenyl)-2-methylpyrido[2,3-d]-pyrimidin-7-yl]-N'-N-dimethylguanidine (77206-79-2)

Guidance literature:

With methylamine; In ethanol;

upstream raw materials:

6-(2,6-dichlorophenyl)-2-methylpyrido<2,3-d>pyrimidin-7-amine

methyl thioisocyanate

Downstream raw materials:

C₁₈H₁₅Cl₂N₉

ethyl N-<6-(2,6-dichlorophenyl)-2-methylpyrido<2,3-d>pyrimidin-7-yl>-N'-methylcarbamimidate

N-<6-(2,6-dichlorophenyl)pyrido<2,3-d>pyrimidin-7-yl>-N'-methylguanidine

N-[6-(2,6-Dichloro-phenyl)-2-methyl-pyrido[2,3-d]pyrimidin-7-yl]-N',N''-dimethyl-guanidine

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