((CH₃)3C₆H₂NC₆H₄)2OZrCl₂

Base Information

Chemical Name:((CH₃)3C₆H₂NC₆H₄)2OZrCl₂
CAS No.:278615-15-9
Molecular Formula:C₃₀H₃₀Cl₂N₂OZr
Molecular Weight:596.711
Hs Code.:

((CH<sub>3</sub>)3C<sub>6</sub>H<sub>2</sub>NC<sub>6</sub>H<sub>4</sub>)2OZrCl<sub>2</sub>

Synonyms:((CH₃)3C₆H₂NC₆H₄)2OZrCl₂

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Chemical Property of ((CH₃)3C₆H₂NC₆H₄)2OZrCl₂

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Technology Process of ((CH₃)3C₆H₂NC₆H₄)2OZrCl₂

There total 2 articles about ((CH₃)3C₆H₂NC₆H₄)2OZrCl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 75-77-4
chloro-trimethyl-silane

: 278615-14-8
((CH₃)3C₆H₂NC₆H₄)2OZr(N(CH₃)2)2

: 278615-15-9
((CH₃)3C₆H₂NC₆H₄)2OZrCl₂

Guidance literature:: In toluene; stirred at room temp. under N2 for 24 h; evapd. in vacuo, crystd. from Et2O; elem. anal.;
DOI:10.1021/om0000921

Reference yield:

: 278615-11-5
(mesitylNH-o-C₆H₄)2O

: 278615-15-9
((CH₃)3C₆H₂NC₆H₄)2OZrCl₂

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether

2: toluene

In diethyl ether; toluene;
DOI:10.1021/om0000921

Reference yield: 92.0%

: 278615-15-9
((CH₃)3C₆H₂NC₆H₄)2OZrCl₂

: 100-58-3
phenylmagnesium bromide

: ((CH₃)3C₆H₂NC₆H₄)2OZr(C₆H₅)2

Guidance literature:: In diethyl ether; PhMgBr in Et2O was added to a suspn. of Zr-complex in Et2O at -30 deg Cunder N2, mixt. was stirred at room temp. for 1.5 h; dioxane was added, filtd. through Celite, concd. in vacuo, cooled to -30 deg C overnight, crystals were collected; elem. anal.;
DOI:10.1021/om0000921