(2E)-4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl)-4-phenylbut-2-enyl acetate

Base Information

Chemical Name:(2E)-4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl)-4-phenylbut-2-enyl acetate
CAS No.:1007392-18-8
Molecular Formula:C₁₈H₂₀O₆
Molecular Weight:332.353
Hs Code.:

Synonyms:(2E)-4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl)-4-phenylbut-2-enyl acetate

Suppliers and Price of (2E)-4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl)-4-phenylbut-2-enyl acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2E)-4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl)-4-phenylbut-2-enyl acetate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2E)-4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl)-4-phenylbut-2-enyl acetate

There total 1 articles about (2E)-4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl)-4-phenylbut-2-enyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1214-54-6
5-benzylidene Meldrum's acid

: 121052-08-2,92081-14-6,352201-91-3
(E)-3-(1,1,1-tributylstannyl)-2-propenyl acetate

: 1007392-18-8
(2E)-4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl)-4-phenylbut-2-enyl acetate

Guidance literature:: chloro(1,5-cyclooctadiene)rhodium(I) dimer; In tetrahydrofuran; at 20 ℃; for 6h;
DOI:10.1021/ol702613f

Reference yield: 73.0%

: 1007392-18-8
(2E)-4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl)-4-phenylbut-2-enyl acetate

: 64-17-5
ethanol

: ethyl (1SR,2RS,3RS)-5-oxo-2-phenyl-3-vinylcyclopentanecarboxylate

Guidance literature:: dichloro bis(acetonitrile) palladium(II); at 60 ℃; for 15h;
DOI:10.1021/ol702613f

Reference yield: 60.0%

: 67-56-1
methanol

: 1007392-18-8
(2E)-4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl)-4-phenylbut-2-enyl acetate

: methyl (1SR,2RS,3RS)-5-oxo-2-phenyl-3-vinylcyclopentanecarboxylate

Guidance literature:: With P(p-CH₃OC₆H₄)3; triethylamine; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; In tetrahydrofuran; at 50 ℃; for 8h;
DOI:10.1021/ol702613f