C₂₇H₃₂N₂O₄

Base Information

Chemical Name:C₂₇H₃₂N₂O₄
CAS No.:221207-60-9
Molecular Formula:C₂₇H₃₂N₂O₄
Molecular Weight:448.562
Hs Code.:

C<sub>27</sub>H<sub>32</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:C₂₇H₃₂N₂O₄

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Chemical Property of C₂₇H₃₂N₂O₄

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Technology Process of C₂₇H₃₂N₂O₄

There total 9 articles about C₂₇H₃₂N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: (R)-1-[(4R,5R)-5-((1S,3R,4R)-3-Benzyloxy-7-aza-bicyclo[2.2.1]hept-1-yl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-2-phenyl-ethylamine

: 221207-60-9
C₂₇H₃₂N₂O₄

Guidance literature:: With pyridine; 1,1'-carbonyldiimidazole; In dichloromethane; Ambient temperature;
DOI:10.1016/S0960-894X(98)00659-3

Reference yield:

: 63219-70-5
N-(benzyloxycarbonyl)-D-phenylalaninal

: 221207-60-9
C₂₇H₃₂N₂O₄

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / VCl₃(THF)3, Zn / CH₂Cl₂ / 2.5 h / Ambient temperature

2: 95 percent / camphorsulfonic acid / CH₂Cl₂ / 6 h / Ambient temperature

3: 95 percent / H₂, NH₃ / Pd/C / methanol / 2 h / 760 Torr / Ambient temperature

4: 67 percent / carbonyldiimidazole, pyridine / CH₂Cl₂ / Ambient temperature

With pyridine; Vanadium (III) chloride-(tris-tetrahydrofuran); camphor-10-sulfonic acid; ammonia; hydrogen; 1,1'-carbonyldiimidazole; zinc; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1016/S0960-894X(98)00659-3

Reference yield:

: 100-39-0
benzyl bromide

: 221207-60-9
C₂₇H₃₂N₂O₄

Guidance literature:: Multi-step reaction with 7 steps

1: NaH / dimethylformamide / 2.5 h / Ambient temperature

2: LiBH₄ / diethyl ether / 15 h / Ambient temperature

3: 81 percent / (ClCO)2, Et₃N, DMSO / CH₂Cl₂ / 2 h / -78 - 20 °C

4: 84 percent / VCl₃(THF)3, Zn / CH₂Cl₂ / 2.5 h / Ambient temperature

5: 95 percent / camphorsulfonic acid / CH₂Cl₂ / 6 h / Ambient temperature

6: 95 percent / H₂, NH₃ / Pd/C / methanol / 2 h / 760 Torr / Ambient temperature

7: 67 percent / carbonyldiimidazole, pyridine / CH₂Cl₂ / Ambient temperature

With pyridine; lithium borohydride; oxalyl dichloride; Vanadium (III) chloride-(tris-tetrahydrofuran); camphor-10-sulfonic acid; ammonia; hydrogen; sodium hydride; dimethyl sulfoxide; triethylamine; 1,1'-carbonyldiimidazole; zinc; palladium on activated charcoal; In methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(98)00659-3