2,5-anhydro-6-O-benzoyl-4-deoxy-4-(thymin-1-yl)-L-mannofuranose dimethyl acetal

Base Information

Chemical Name:2,5-anhydro-6-O-benzoyl-4-deoxy-4-(thymin-1-yl)-L-mannofuranose dimethyl acetal
CAS No.:210636-18-3
Molecular Formula:C₂₀H₂₄N₂O₈
Molecular Weight:420.419
Hs Code.:

Synonyms:2,5-anhydro-6-O-benzoyl-4-deoxy-4-(thymin-1-yl)-L-mannofuranose dimethyl acetal

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Chemical Property of 2,5-anhydro-6-O-benzoyl-4-deoxy-4-(thymin-1-yl)-L-mannofuranose dimethyl acetal

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Technology Process of 2,5-anhydro-6-O-benzoyl-4-deoxy-4-(thymin-1-yl)-L-mannofuranose dimethyl acetal

There total 1 articles about 2,5-anhydro-6-O-benzoyl-4-deoxy-4-(thymin-1-yl)-L-mannofuranose dimethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 98-88-4
benzoyl chloride

: 196596-85-7
2,5-anhdyro-4-deoxy-4-(thymin-1-yl)-L-mannofuranose dimethyl acetal

: 210636-18-3
2,5-anhydro-6-O-benzoyl-4-deoxy-4-(thymin-1-yl)-L-mannofuranose dimethyl acetal

Guidance literature:: With pyridine; at 20 ℃; for 28h;
DOI:10.1002/(SICI)1522-2675(19991110)82:11<2037::AID-HLCA2037>3.0.CO;2-I

Reference yield: 97.0%

: 210636-18-3
2,5-anhydro-6-O-benzoyl-4-deoxy-4-(thymin-1-yl)-L-mannofuranose dimethyl acetal

: 258524-62-8
2,5-anhydro-1-O-benzoyl-3-deoxy-3-(thymin-1-yl)-L-mannitol

Guidance literature:: With water; trifluoroacetic acid; In tetrahydrofuran; for 26h; Heating;
DOI:10.1002/(SICI)1522-2675(19991110)82:11<2037::AID-HLCA2037>3.0.CO;2-I

Reference yield:

: 210636-18-3
2,5-anhydro-6-O-benzoyl-4-deoxy-4-(thymin-1-yl)-L-mannofuranose dimethyl acetal

: 258524-67-3
2,5-anhydro-1-O-benzoyl-3-deoxy-5-O-(dimethoxytrityl)-3-(thymin-1-yl)-L-mannitol

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / H₂O; CF₃COOH / tetrahydrofuran / 26 h / Heating

2: 77 percent / pyridine / 26 h / 20 °C

With pyridine; water; trifluoroacetic acid; In tetrahydrofuran; 1: Hydrolysis / 2: Etherification;
DOI:10.1002/(SICI)1522-2675(19991110)82:11<2037::AID-HLCA2037>3.0.CO;2-I