N-[2-(N,N-dimethylamino)phenyl]-2-[(phenylmethoxy)carbonylamino]ethanamide

Base Information

• Chemical Name: N-[2-(N,N-dimethylamino)phenyl]-2-[(phenylmethoxy)carbonylamino]ethanamide
• CAS No.: 696605-19-3
• Molecular Formula: C₁₈H₂₁N₃O₃
• Molecular Weight: 327.383

Synonyms:N-[2-(N,N-dimethylamino)phenyl]-2-[(phenylmethoxy)carbonylamino]ethanamide

Chemical Property of N-[2-(N,N-dimethylamino)phenyl]-2-[(phenylmethoxy)carbonylamino]ethanamide

Chemical Property:

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Technology Process of N-[2-(N,N-dimethylamino)phenyl]-2-[(phenylmethoxy)carbonylamino]ethanamide

There total 2 articles about N-[2-(N,N-dimethylamino)phenyl]-2-[(phenylmethoxy)carbonylamino]ethanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

N,N-dimethyl-1,2-phenylenediamine (2836-03-5) + N-(Benzyloxycarbonyl)glycine (1138-80-3) → N-[2-(N,N-dimethylamino)phenyl]-2-[(phenylmethoxy)carbonylamino]ethanamide (696605-19-3)

Guidance literature:

With dicyclohexyl-carbodiimide; In tetrahydrofuran; at 20 ℃; for 6h;

DOI:10.1039/b313996d

Reference yield:

N-(2-N,N-dimethylaminophenyl)-1,1-dimethylethyl ester carbamic acid (696604-98-5) → N-[2-(N,N-dimethylamino)phenyl]-2-[(phenylmethoxy)carbonylamino]ethanamide (696605-19-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 68 percent / trifluoroacetic acid / CH₂Cl₂ / 1 h / 20 °C

2: 71 percent / dicyclohexylcarbodiimide / tetrahydrofuran / 6 h / 20 °C

With dicyclohexyl-carbodiimide; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;

DOI:10.1039/b313996d

Reference yield: 81.0%

N-[2-(N,N-dimethylamino)phenyl]-2-[(phenylmethoxy)carbonylamino]ethanamide (696605-19-3) → 2-amino-N-[2-(N,N-dimethylamino)phenyl]ethanamide (696605-41-1)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; for 2h; atmospheric pressure;

DOI:10.1039/b313996d

upstream raw materials:

N,N-dimethyl-1,2-phenylenediamine

N-(Benzyloxycarbonyl)glycine

N-(2-N,N-dimethylaminophenyl)-1,1-dimethylethyl ester carbamic acid

Downstream raw materials:

2-amino-N-[2-(N,N-dimethylamino)phenyl]ethanamide

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