(6R,9aS)-2-benzyl-6-(4-methoxy-2,3-dimethylphenyl)-octahydro-pyrido[1,2-a]pyrazine

Base Information

Chemical Name:(6R,9aS)-2-benzyl-6-(4-methoxy-2,3-dimethylphenyl)-octahydro-pyrido[1,2-a]pyrazine
CAS No.:869794-16-1
Molecular Formula:C₂₄H₃₂N₂O
Molecular Weight:364.531
Hs Code.:

Synonyms:(6R,9aS)-2-benzyl-6-(4-methoxy-2,3-dimethylphenyl)-octahydro-pyrido[1,2-a]pyrazine

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Chemical Property of (6R,9aS)-2-benzyl-6-(4-methoxy-2,3-dimethylphenyl)-octahydro-pyrido[1,2-a]pyrazine

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Technology Process of (6R,9aS)-2-benzyl-6-(4-methoxy-2,3-dimethylphenyl)-octahydro-pyrido[1,2-a]pyrazine

There total 8 articles about (6R,9aS)-2-benzyl-6-(4-methoxy-2,3-dimethylphenyl)-octahydro-pyrido[1,2-a]pyrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₁H₃₈N₄O₃S

: 869794-16-1
(6R,9aS)-2-benzyl-6-(4-methoxy-2,3-dimethylphenyl)-octahydro-pyrido[1,2-a]pyrazine

Guidance literature:: C₃₁H₃₈N₄O₃S; With zinc trifluoromethanesulfonate; sodium cyanoborohydride; In tetrahydrofuran; methanol; at 65 ℃; for 5.5h;

With sodium hydrogencarbonate; In tetrahydrofuran; methanol; water; for 0.5h;

Reference yield:

: C₃₁H₃₈N₄O₃S

: 869794-16-1
(6R,9aS)-2-benzyl-6-(4-methoxy-2,3-dimethylphenyl)-octahydro-pyrido[1,2-a]pyrazine

Guidance literature:: C₃₁H₃₈N₄O₃S; With zinc trifluoromethanesulfonate; sodium cyanoborohydride; In methanol; at 65 ℃; for 6h;

With sodium hydrogencarbonate; In methanol; water; for 0.5h;

Reference yield:

: 869794-14-9
(E)-1-((S)-4-Benzyl-piperazin-2-yl)-4-(4-methoxy-2,3-dimethylphenyl)-but-3-en-2-one

: 869794-16-1
(6R,9aS)-2-benzyl-6-(4-methoxy-2,3-dimethylphenyl)-octahydro-pyrido[1,2-a]pyrazine

Guidance literature:: Multi-step reaction with 3 steps

1.1: ammonium acetate / methanol; water / 16.5 h / 20 - 60 °C

2.1: tetrahydrofuran; methanol / 20.5 h / 20 °C

3.1: zinc trifluoromethanesulfonate; sodium cyanoborohydride / tetrahydrofuran; methanol / 5.5 h / 65 °C

3.2: 0.5 h

With ammonium acetate; zinc trifluoromethanesulfonate; sodium cyanoborohydride; In tetrahydrofuran; methanol; water;