5,5'-dimethyl-2,2'-diphenyl-1,2,1',2'-tetrahydro-4,4'-methanediyl-bis-pyrazol-3-one

Base Information

• Chemical Name: 5,5'-dimethyl-2,2'-diphenyl-1,2,1',2'-tetrahydro-4,4'-methanediyl-bis-pyrazol-3-one
• CAS No.: 172038-40-3
• Molecular Formula: C₂₁H₂₀N₄O₂
• Molecular Weight: 360.415

Synonyms:5,5'-dimethyl-2,2'-diphenyl-1,2,1',2'-tetrahydro-4,4'-methanediyl-bis-pyrazol-3-one

Chemical Property of 5,5'-dimethyl-2,2'-diphenyl-1,2,1',2'-tetrahydro-4,4'-methanediyl-bis-pyrazol-3-one

Chemical Property:

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Technology Process of 5,5'-dimethyl-2,2'-diphenyl-1,2,1',2'-tetrahydro-4,4'-methanediyl-bis-pyrazol-3-one

There total 10 articles about 5,5'-dimethyl-2,2'-diphenyl-1,2,1',2'-tetrahydro-4,4'-methanediyl-bis-pyrazol-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-methyl-1-phenylpyrazolin-5(4H)-one (19735-89-8) + sodium methylate (124-41-4) → (5-methyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-(3-methyl-5-oxo-1-phenyl-1,5-dihydro-pyrazol-4-ylidene)-methane (15900-11-5) + 5,5'-dimethyl-2,2'-diphenyl-1,2,1',2'-tetrahydro-4,4'-methanediyl-bis-pyrazol-3-one (172038-40-3)

Guidance literature:

With bis(1-chloroethyl) sulfide;

DOI:10.1097/00005537-200203000-00005

Reference yield:

3-methyl-1-phenylpyrazolin-5(4H)-one (19735-89-8) + formamide (77287-34-4,77287-35-5,60100-09-6) → (5-methyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-(3-methyl-5-oxo-1-phenyl-1,5-dihydro-pyrazol-4-ylidene)-methane (15900-11-5) + 5,5'-dimethyl-2,2'-diphenyl-1,2,1',2'-tetrahydro-4,4'-methanediyl-bis-pyrazol-3-one (172038-40-3)

Guidance literature:

Reference yield:

3-methyl-1-phenylpyrazolin-5(4H)-one (19735-89-8) → 5,5'-dimethyl-2,2'-diphenyl-1,2,1',2'-tetrahydro-4,4'-methanediyl-bis-pyrazol-3-one (172038-40-3)

Guidance literature:

Multi-step reaction with 2 steps

2: zinc; acetic acid

With acetic acid; zinc;

upstream raw materials:

formaldehyd

3-methyl-1-phenylpyrazolin-5(4H)-one

sodium methylate

formamide

Downstream raw materials:

5,5'-diacetoxy-3,3'-dimethyl-1,1'-diphenyl-1H,1'H-4,4'-methanediyl-bis-pyrazole

3-methyl-1-phenylpyrazole-4,5-dione 4-phenylhydrazone

(5-methyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-(3-methyl-5-oxo-1-phenyl-1,5-dihydro-pyrazol-4-ylidene)-methane

4,10-dimethyl-2,8-diphenyl-2,3,8,9-tetraaza-dispiro[4.0.4.1]undeca-3,9-diene-1,7-dione

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