6-(2,3-dimethoxy-4-isopropylbenzyl)-2,2-dimethyl-3,3-ethylenedioxycyclohexanone

Base Information

Chemical Name:6-(2,3-dimethoxy-4-isopropylbenzyl)-2,2-dimethyl-3,3-ethylenedioxycyclohexanone
CAS No.:182689-73-2
Molecular Formula:C₂₂H₃₂O₅
Molecular Weight:376.493
Hs Code.:

Synonyms:6-(2,3-dimethoxy-4-isopropylbenzyl)-2,2-dimethyl-3,3-ethylenedioxycyclohexanone

Suppliers and Price of 6-(2,3-dimethoxy-4-isopropylbenzyl)-2,2-dimethyl-3,3-ethylenedioxycyclohexanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 6-(2,3-dimethoxy-4-isopropylbenzyl)-2,2-dimethyl-3,3-ethylenedioxycyclohexanone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 6-(2,3-dimethoxy-4-isopropylbenzyl)-2,2-dimethyl-3,3-ethylenedioxycyclohexanone

There total 4 articles about 6-(2,3-dimethoxy-4-isopropylbenzyl)-2,2-dimethyl-3,3-ethylenedioxycyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 146725-00-0
2,3-dimethoxy-4-isopropylphenylmethyl bromide

: 14782-52-6
ethylene glycole monoacetal of 2,2-dimethylcyclohexane-1,3-dione

: 182689-73-2
6-(2,3-dimethoxy-4-isopropylbenzyl)-2,2-dimethyl-3,3-ethylenedioxycyclohexanone

Guidance literature:: With potassium hydride; In tetrahydrofuran; for 24h; Ambient temperature;

Reference yield:

: 562-13-0
2,2-dimethyl-1,3-cyclohexanedione

: 182689-73-2
6-(2,3-dimethoxy-4-isopropylbenzyl)-2,2-dimethyl-3,3-ethylenedioxycyclohexanone

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / BF₃*Et₂O / diethyl ether / 24 h / Ambient temperature

2: 86 percent / KH / tetrahydrofuran / 24 h / Ambient temperature

With boron trifluoride diethyl etherate; potassium hydride; In tetrahydrofuran; diethyl ether;

Reference yield:

: 71720-27-9
3-Isopropyl-veratrol

: 182689-73-2
6-(2,3-dimethoxy-4-isopropylbenzyl)-2,2-dimethyl-3,3-ethylenedioxycyclohexanone

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-BuLi / 1.) THF, ether, rt, 5 h, 2.) THF, ether, rt, overnight

2: 97 percent / PBr₃ / CH₂Cl₂ / 1 h / Ambient temperature

3: 86 percent / KH / tetrahydrofuran / 24 h / Ambient temperature

With n-butyllithium; phosphorus tribromide; potassium hydride; In tetrahydrofuran; dichloromethane;