8-(4-isopropyl-2,3-dimethoxy-benzyl)-6,6-dimethyl-7-vinyl-1,4-dioxa-spiro[4.5]decan-7-ol

Base Information

Chemical Name:8-(4-isopropyl-2,3-dimethoxy-benzyl)-6,6-dimethyl-7-vinyl-1,4-dioxa-spiro[4.5]decan-7-ol
CAS No.:1026465-43-9
Molecular Formula:C₂₄H₃₆O₅
Molecular Weight:404.547
Hs Code.:

Synonyms:8-(4-isopropyl-2,3-dimethoxy-benzyl)-6,6-dimethyl-7-vinyl-1,4-dioxa-spiro[4.5]decan-7-ol

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Chemical Property of 8-(4-isopropyl-2,3-dimethoxy-benzyl)-6,6-dimethyl-7-vinyl-1,4-dioxa-spiro[4.5]decan-7-ol

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Technology Process of 8-(4-isopropyl-2,3-dimethoxy-benzyl)-6,6-dimethyl-7-vinyl-1,4-dioxa-spiro[4.5]decan-7-ol

There total 6 articles about 8-(4-isopropyl-2,3-dimethoxy-benzyl)-6,6-dimethyl-7-vinyl-1,4-dioxa-spiro[4.5]decan-7-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 562-13-0
2,2-dimethyl-1,3-cyclohexanedione

: 1026465-43-9
8-(4-isopropyl-2,3-dimethoxy-benzyl)-6,6-dimethyl-7-vinyl-1,4-dioxa-spiro[4.5]decan-7-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / BF₃*Et₂O / diethyl ether / 24 h / Ambient temperature

2: 86 percent / KH / tetrahydrofuran / 24 h / Ambient temperature

3: tetrahydrofuran / 1 h / Ambient temperature

With boron trifluoride diethyl etherate; potassium hydride; In tetrahydrofuran; diethyl ether;

Reference yield:

: 71720-27-9
3-Isopropyl-veratrol

: 1026465-43-9
8-(4-isopropyl-2,3-dimethoxy-benzyl)-6,6-dimethyl-7-vinyl-1,4-dioxa-spiro[4.5]decan-7-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) n-BuLi / 1.) THF, ether, rt, 5 h, 2.) THF, ether, rt, overnight

2: 97 percent / PBr₃ / CH₂Cl₂ / 1 h / Ambient temperature

3: 86 percent / KH / tetrahydrofuran / 24 h / Ambient temperature

4: tetrahydrofuran / 1 h / Ambient temperature

With n-butyllithium; phosphorus tribromide; potassium hydride; In tetrahydrofuran; dichloromethane;

Reference yield:

: 146725-00-0
2,3-dimethoxy-4-isopropylphenylmethyl bromide

: 1026465-43-9
8-(4-isopropyl-2,3-dimethoxy-benzyl)-6,6-dimethyl-7-vinyl-1,4-dioxa-spiro[4.5]decan-7-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / KH / tetrahydrofuran / 24 h / Ambient temperature

2: tetrahydrofuran / 1 h / Ambient temperature

With potassium hydride; In tetrahydrofuran;