[4-(6-chloro-5-cyanopyrazine-2-yl)phenyl]aminoformic acid tert-butyl ester

Base Information

Chemical Name:[4-(6-chloro-5-cyanopyrazine-2-yl)phenyl]aminoformic acid tert-butyl ester
CAS No.:1426214-88-1
Molecular Formula:C₁₆H₁₅ClN₄O₂
Molecular Weight:330.774
Hs Code.:

Synonyms:[4-(6-chloro-5-cyanopyrazine-2-yl)phenyl]aminoformic acid tert-butyl ester

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Chemical Property of [4-(6-chloro-5-cyanopyrazine-2-yl)phenyl]aminoformic acid tert-butyl ester

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Technology Process of [4-(6-chloro-5-cyanopyrazine-2-yl)phenyl]aminoformic acid tert-butyl ester

There total 1 articles about [4-(6-chloro-5-cyanopyrazine-2-yl)phenyl]aminoformic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 313339-92-3
3,5-dichloro-pyrazine-2-carbonitrile

: 330793-01-6
(4-tert-butoxycarbonylaminophenyl)boronic acid pinacol ester

: 1426214-88-1
[4-(6-chloro-5-cyanopyrazine-2-yl)phenyl]aminoformic acid tert-butyl ester

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate; In 1,4-dioxane; water; at 100 ℃; for 1h;

Reference yield: 83.0%

: 1426214-88-1
[4-(6-chloro-5-cyanopyrazine-2-yl)phenyl]aminoformic acid tert-butyl ester

: 1426214-89-2
[4-(3-amino-1H-pyrazolo[3,4-b]pyrazin-6-yl)-phenyl]-carbamic acid tert-butyl ester

Guidance literature:: With hydrazine; In water; isopropyl alcohol; at 120 ℃; for 1.16667h; Microwave irradiation; Sealed tube;

Reference yield:

: 1426214-88-1
[4-(6-chloro-5-cyanopyrazine-2-yl)phenyl]aminoformic acid tert-butyl ester

: 1426215-67-9
C₁₁H₁₀N₆

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine / water; isopropyl alcohol / 1.17 h / 20 - 120 °C

2: hydrogenchloride / 1,4-dioxane; water / 2 h / 20 - 25 °C

With hydrogenchloride; hydrazine; In 1,4-dioxane; water; isopropyl alcohol;