((4-methoxybenzyl)imino)(methyl)(phenyl)-λ⁶-sulfanone

Base Information

Chemical Name:((4-methoxybenzyl)imino)(methyl)(phenyl)-λ⁶-sulfanone
CAS No.:1202255-11-5
Molecular Formula:C₁₅H₁₇NO₂S
Molecular Weight:275.371
Hs Code.:

((4-methoxybenzyl)imino)(methyl)(phenyl)-λ<sup>6</sup>-sulfanone

Synonyms:((4-methoxybenzyl)imino)(methyl)(phenyl)-λ⁶-sulfanone

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Chemical Property of ((4-methoxybenzyl)imino)(methyl)(phenyl)-λ⁶-sulfanone

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Technology Process of ((4-methoxybenzyl)imino)(methyl)(phenyl)-λ⁶-sulfanone

There total 3 articles about ((4-methoxybenzyl)imino)(methyl)(phenyl)-λ⁶-sulfanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 2746-25-0
p-Methoxybenzyl bromide

: 4381-25-3
S-methyl-S-phenylsulfoximine

: 1202255-11-5
((4-methoxybenzyl)imino)(methyl)(phenyl)-λ⁶-sulfanone

Guidance literature:: S-methyl-S-phenylsulfoximine; With tetrabutylammomium bromide; potassium hydride; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;

p-Methoxybenzyl bromide; In tetrahydrofuran; for 2h; Inert atmosphere;
DOI:10.1002/anie.201203258

Reference yield: 91.0%

: N-(4-methoxybenzyl)benzenesulfonimidoyl fluoride

: 917-54-4
methyllithium

: 1202255-11-5
((4-methoxybenzyl)imino)(methyl)(phenyl)-λ⁶-sulfanone

Guidance literature:: In tetrahydrofuran; at -78 ℃; for 0.166667h; Sealed tube; Inert atmosphere;
DOI:10.1002/anie.201712145

Reference yield:

: 2393-23-9
4-methoxy-benzylamine

: 1202255-11-5
((4-methoxybenzyl)imino)(methyl)(phenyl)-λ⁶-sulfanone

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine; thionyl tetrafluoride / dichloromethane / 0.5 h / 20 °C / Sealed tube

2: dibutyl ether / 0.08 h / -78 °C / Sealed tube; Inert atmosphere

3: tetrahydrofuran / 0.17 h / -78 °C / Sealed tube; Inert atmosphere

With thionyl tetrafluoride; triethylamine; In tetrahydrofuran; dichloromethane; dibutyl ether;
DOI:10.1002/anie.201712145