2,4-Dichloro-1-(2-iodophenoxy)benzene

Base Information

Chemical Name:2,4-Dichloro-1-(2-iodophenoxy)benzene
CAS No.:175136-78-4
Molecular Formula:C12H7 Cl2 I O
Molecular Weight:364.99
Hs Code.:2909309090
DSSTox Substance ID:DTXSID50380324
Wikidata:Q82170516
Mol file:175136-78-4.mol

Synonyms:2,4-dichloro-1-(2-iodophenoxy)benzene;175136-78-4;Benzene, 2,4-dichloro-1-(2-iodophenoxy)-;DTXSID50380324;MFCD00052444;AKOS015908930;2,4-Dichloro-1(2-iodophenoxy)benzene;MS-22032;FT-0609998

Suppliers and Price of 2,4-Dichloro-1-(2-iodophenoxy)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2,4-DICHLORO-1-(2-IODOPHENOXY)BENZENE 95.00%
50G
$ 3196.81

American Custom Chemicals Corporation
2,4-DICHLORO-1-(2-IODOPHENOXY)BENZENE 95.00%
10G
$ 1301.29

American Custom Chemicals Corporation
2,4-DICHLORO-1-(2-IODOPHENOXY)BENZENE 95.00%
1G
$ 670.66

Total 9 raw suppliers

Chemical Property of 2,4-Dichloro-1-(2-iodophenoxy)benzene

Chemical Property:

Vapor Pressure:0.000125mmHg at 25°C
Boiling Point:345.1°Cat760mmHg
Flash Point:162.5°C
PSA：9.23000
Density:1.771g/cm³
LogP:5.39030
XLogP3:6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:363.89187
Heavy Atom Count:16
Complexity:227

Purity/Quality:

98%Min ^*data from raw suppliers

2,4-DICHLORO-1-(2-IODOPHENOXY)BENZENE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s): R36/37/38:Irritating to eyes, respiratory system and skin.;
Hazard Codes: Xi:Irritant;
Statements: R36/37/38:Irritating to eyes, respiratory system and skin.;
Safety Statements: S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.; S37/39:Wear suitable g

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)OC2=C(C=C(C=C2)Cl)Cl)I

Technology Process of 2,4-Dichloro-1-(2-iodophenoxy)benzene

There total 1 articles about 2,4-Dichloro-1-(2-iodophenoxy)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 26306-64-9
2,4-dichloro-1-(2-aminophenoxy)benzene

: 175136-78-4
2,4-dichloro-1-(2-iodophenoxy)benzene

Guidance literature:: 2,4-dichloro-1-(2-aminophenoxy)benzene; With sulfuric acid; sodium nitrite; In water; at 0 - 5 ℃; for 0.166667h;

With potassium iodide; In water; at 0 - 20 ℃; for 4.5h;
DOI:10.1002/cmdc.201400058

Reference yield: 78.0%

: 121-43-7,63156-11-6
Trimethyl borate

: 175136-78-4
2,4-dichloro-1-(2-iodophenoxy)benzene

: 163517-60-0
2-(2,4-dichlorophenoxy)phenylboronic acid

Guidance literature:: 2,4-dichloro-1-(2-iodophenoxy)benzene; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

Trimethyl borate; In tetrahydrofuran; at -78 - 20 ℃; for 3h; Inert atmosphere;

With hydrogenchloride; In tetrahydrofuran; at 20 ℃;
DOI:10.1002/cmdc.201400058

Reference yield:

: 175136-78-4
2,4-dichloro-1-(2-iodophenoxy)benzene

: 1519044-07-5
tert-butyl 2-(3-(2-(2,4-dichlorophenoxy)phenyl)thiophene-2-sulfonamido)ethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

1.2: 3 h / -78 - 20 °C / Inert atmosphere

1.3: 20 °C

2.1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; palladium diacetate / tetrahydrofuran / 8 h / Inert atmosphere; Reflux

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; n-butyllithium; palladium diacetate; In tetrahydrofuran; 2.1: |Suzuki Coupling;
DOI:10.1002/cmdc.201400058