2-hydroxy-3,6-dimethylbenzoic acid methyl ester

Base Information

Chemical Name:2-hydroxy-3,6-dimethylbenzoic acid methyl ester
CAS No.:3921-13-9
Molecular Formula:C₁₀H₁₂O₃
Molecular Weight:180.203
Hs Code.:

Synonyms:2-hydroxy-3,6-dimethylbenzoic acid methyl ester

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Chemical Property of 2-hydroxy-3,6-dimethylbenzoic acid methyl ester

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Technology Process of 2-hydroxy-3,6-dimethylbenzoic acid methyl ester

There total 6 articles about 2-hydroxy-3,6-dimethylbenzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: methyl (E)-4-methyl-3-oxooct-6-enoate

: 3921-13-9
2-hydroxy-3,6-dimethylbenzoic acid methyl ester

Guidance literature:: With oxygen; copper diacetate; palladium diacetate; In dimethyl sulfoxide; at 45 ℃; for 23h; under 760.051 Torr; chemoselective reaction;
DOI:10.1016/j.tetlet.2019.05.041

Reference yield: 40.0%

: 4652-27-1
4-methoxy-3-buten-2-one

: 78133-88-7
1,3-bis(trimethylsiloxy)-1-methoxypenta-1,3-diene

: 3921-13-9
2-hydroxy-3,6-dimethylbenzoic acid methyl ester

Guidance literature:: 4-methoxy-3-buten-2-one; 1,3-bis(trimethylsiloxy)-1-methoxypenta-1,3-diene; With titanium tetrachloride; In dichloromethane; at -78 - 20 ℃; for 14h; Inert atmosphere;

With hydrogenchloride; water; In dichloromethane; regioselective reaction; Inert atmosphere;
DOI:10.1055/s-0029-1216814

Reference yield: 25.0%

: 13730-55-7
methyl 2,5-dimethylbenzoate

: 27023-05-8
methyl 4-hydroxy-2,5-dimethylbenzoate

: 27023-04-7
methyl 3-hydroxy-2,5-dimethylbenzoate

: 3921-13-9
2-hydroxy-3,6-dimethylbenzoic acid methyl ester

Guidance literature:: methyl 2,5-dimethylbenzoate; With 6,7-dichlorobenzo[d][1,2]dioxine-1,4-dione; at 75 ℃; for 48h;

With water; sodium hydrogencarbonate; In methanol; at 50 ℃; for 1h; Overall yield = 51 %; regioselective reaction; Inert atmosphere;
DOI:10.1021/acs.joc.5b01079