N,N-diphenoxycarbonyl-6-(4-amino-2,3-dichlorophenoxy)pyrimidin-4-amine

Base Information Edit

Chemical Name:N,N-diphenoxycarbonyl-6-(4-amino-2,3-dichlorophenoxy)pyrimidin-4-amine
CAS No.:1337932-35-0
Molecular Formula:C₂₄H₁₆Cl₂N₄O₅
Molecular Weight:511.321
Hs Code.:
Mol file:1337932-35-0.mol

Synonyms:N,N-diphenoxycarbonyl-6-(4-amino-2,3-dichlorophenoxy)pyrimidin-4-amine

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Chemical Property of N,N-diphenoxycarbonyl-6-(4-amino-2,3-dichlorophenoxy)pyrimidin-4-amine Edit

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Technology Process of N,N-diphenoxycarbonyl-6-(4-amino-2,3-dichlorophenoxy)pyrimidin-4-amine

There total 2 articles about N,N-diphenoxycarbonyl-6-(4-amino-2,3-dichlorophenoxy)pyrimidin-4-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1337932-19-0
6-(2,3-dichloro-4-nitrophenoxy)pyrimidin-4-amine

: 1885-14-9
phenyl chloroformate

: 1337932-35-0
N,N-diphenoxycarbonyl-6-(4-amino-2,3-dichlorophenoxy)pyrimidin-4-amine

Guidance literature:: 6-(2,3-dichloro-4-nitrophenoxy)pyrimidin-4-amine; phenyl chloroformate; With triethylamine; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;

With iron; acetic acid; at 60 ℃; for 1.5h;

With sodium hydrogencarbonate; In water;

Reference yield:

: 36556-51-1
2,3-dichloro-1-fluoro-4-nitrobenzene

: 1337932-35-0
N,N-diphenoxycarbonyl-6-(4-amino-2,3-dichlorophenoxy)pyrimidin-4-amine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dimethyl sulfoxide / 1.5 h / 20 °C

1.2: 16 h

2.1: triethylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

2.2: 1.5 h / 60 °C

With 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In dichloromethane; dimethyl sulfoxide;