N-(4-acetyl-6-chloropyridin-3-yl)-4-nitro-N-(4-nitrophenylsulfonyl)benzenesulfonamide

Base Information

Chemical Name:N-(4-acetyl-6-chloropyridin-3-yl)-4-nitro-N-(4-nitrophenylsulfonyl)benzenesulfonamide
CAS No.:1214241-94-7
Molecular Formula:C₁₉H₁₃ClN₄O₉S₂
Molecular Weight:540.919
Hs Code.:

Synonyms:N-(4-acetyl-6-chloropyridin-3-yl)-4-nitro-N-(4-nitrophenylsulfonyl)benzenesulfonamide

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Chemical Property of N-(4-acetyl-6-chloropyridin-3-yl)-4-nitro-N-(4-nitrophenylsulfonyl)benzenesulfonamide

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Technology Process of N-(4-acetyl-6-chloropyridin-3-yl)-4-nitro-N-(4-nitrophenylsulfonyl)benzenesulfonamide

There total 6 articles about N-(4-acetyl-6-chloropyridin-3-yl)-4-nitro-N-(4-nitrophenylsulfonyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1214241-92-5
1-(5-amino-2-chloropyridin-4-yl)ethanone

: 98-74-8
4-Nitrobenzenesulfonyl chloride

: 1214241-94-7
N-(4-acetyl-6-chloropyridin-3-yl)-4-nitro-N-(4-nitrophenylsulfonyl)benzenesulfonamide

Guidance literature:: 1-(5-amino-2-chloropyridin-4-yl)ethanone; 4-Nitrobenzenesulfonyl chloride; With pyridine; at 20 ℃; for 18h;

With water; Cooling with ice;

Reference yield:

: 1214241-85-6
(E)-2-(2-chloro-5-nitropyridin-4-yl)-N,N-dimethylethenamine

: 1214241-94-7
N-(4-acetyl-6-chloropyridin-3-yl)-4-nitro-N-(4-nitrophenylsulfonyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium periodate / water; tetrahydrofuran / 6 h / 20 °C

2.1: titanium tetrachloride / dichloromethane; diethyl ether / 1 h / -78 - -50 °C

2.2: 1 h / -50 °C

3.1: Dess-Martin periodane / dichloromethane / 16 h

4.1: acetic acid; iron / 4 h

5.1: pyridine / 18 h / 20 °C

5.2: Cooling with ice

With pyridine; sodium periodate; titanium tetrachloride; iron; Dess-Martin periodane; acetic acid; In tetrahydrofuran; diethyl ether; dichloromethane; water;

Reference yield:

: 1214241-89-0
1-(2-chloro-5-nitropyridin-4-yl)ethanol

: 1214241-94-7
N-(4-acetyl-6-chloropyridin-3-yl)-4-nitro-N-(4-nitrophenylsulfonyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: Dess-Martin periodane / dichloromethane / 16 h

2.1: acetic acid; iron / 4 h

3.1: pyridine / 18 h / 20 °C

3.2: Cooling with ice

With pyridine; iron; Dess-Martin periodane; acetic acid; In dichloromethane;